Series type TiN/TiO2 composite film and preparation method and application thereof

A composite thin-film, tandem-type technology, which is applied to the device and coating of the surface coating liquid, can solve the problems of easy hydrolysis and oxidation, harsh experimental conditions, and danger, and achieve high-efficiency photocatalytic performance and excellent hydrophilicity performance effect

Active Publication Date: 2019-06-04
ZHEJIANG UNIV
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  • Abstract
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Problems solved by technology

However, the precursors used to prepare TiN thin films by chemical methods are mostly titanium amide complexes, which are easily hydrolyzed and oxidized in air and moisture. During the preparation and heat treatment of thin films, the reaction environment requires low oxygen content, and some require NH 3 Atmosphere or N 2 Atmosphere, harsh experimental conditions and certain dangers, not suitable for low-cost large-scale production

Method used

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  • Series type TiN/TiO2 composite film and preparation method and application thereof
  • Series type TiN/TiO2 composite film and preparation method and application thereof
  • Series type TiN/TiO2 composite film and preparation method and application thereof

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Embodiment Construction

[0042] The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments. It should be understood that these examples are only used to illustrate the present invention and are not intended to limit the scope of the present invention. For the experimental methods without specific conditions indicated in the following examples, the conventional conditions or the conditions suggested by the manufacturer are usually followed.

[0043] (1) The glass substrate was ultrasonically cleaned with surfactant, ethanol, and water for 30 minutes, and then vacuum-dried at 80°C.

[0044] (2) Dispersion aid Tween 80 (C 12 h 10 CINO 3 ) was mixed with TiN powder at a mass percentage of 3%, ball milled for 24 hours, and taken out for use.

[0045] (3) Dispersion aid Tween 80 is dispersed in deionized water with 3% by mass percent of TiN powder after ball milling, and the configuration concentration is 0.2mol L -1 TiN aqueous dispersi...

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Abstract

The invention discloses a preparation method of a series type TiN / TiO2 composite film, the preparation method comprises the following steps: dispersing TiN nano powder and a dispersing aid in deionized water, adjusting the pH to be larger than 6, and performing ultrasonic treatment to obtain a TiN coating precursor sol; heating a clean substrate to be not lower than 100 DEG C, spraying the TiN coating precursor sol obtained by ultrasonic atomization on the surface of the heated substrate, and cooling to obtain a TiN film; and annealing the obtained TiN film to obtain the series type TiN / TiO2 composite film. The invention also discloses the series type TiN / TiO2 composite film prepared by the preparation method and application thereof in a glass coating layer. The hydrophilicity and photocatalytic properties of the series type TiN / TiO2 composite film are controllable, and the performance of plated glass can be effectively controlled after plating of the series type TiN / TiO2 composite film on the glass.

Description

technical field [0001] The invention relates to the field of composite thin films, in particular to a tandem TiN / TiO 2 Composite film and its preparation method and application. Background technique [0002] my country is a big energy-consuming country, among which the energy consumption of buildings accounts for nearly 40% of the total energy consumption of the whole society, and it shows an increasing trend year by year. In a narrow sense, building energy consumption refers to the daily energy consumption of buildings, including heating, air conditioning, lighting, etc. Glass is the main lighting material for buildings and has become an indispensable material for modern architecture. However, more than 95% of the building area in our country is made of ordinary glass. This type of glass has good light transmission, but it cannot prevent the heat of sunlight from radiating into the building and the heat in the building from diffusing to the outside, which cannot achieve t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C17/25C03C17/27C03C17/22B05D7/24B05D1/02
Inventor 刘涌陈胜男韩高荣汪建勋徐刚
Owner ZHEJIANG UNIV
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