Preparation method of echinoid titanium dioxide microspheres in single/double layer cavity structure
A titanium dioxide, single-layer technology, applied in the direction of titanium dioxide, titanium oxide/hydroxide, etc., can solve the problems such as no titanium dioxide cavity microspheres reported, and achieve high yield, low preparation cost, and controllable process flow Effect
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example 1
[0027] Step 1: Preparation of monodisperse silica microspheres using Method, in a mixture of tetraethyl orthosilicate, absolute ethanol and deionized water, under room temperature (20°C-30°C), magnetic stirring, adding catalyst ammonia water (concentration: 25%-28%), reaction 6 hours, centrifuged, washed with water, and dried to obtain silica microspheres with a diameter of about 300 nm. The molar ratio of each material is: ethyl orthosilicate: ammonia water: water: absolute ethanol = 1: 14: 135: 86.
[0028] Step 2: Disperse the silica microspheres in water for ultrasonic activation, centrifuge, disperse in a large amount of absolute ethanol, add a certain amount of catalyst ammonia water (concentration is 25%-28%), ultrasonically disperse, heat in a water bath at 45°C, and magnetically Stir, and finally add tetrabutyl titanate ethanol solution, react for 2 hours, centrifuge, wash with alcohol, wash with water, and dry to obtain silica / titanium oxide core-shell composite mi...
example 2
[0032] Step 1: Preparation of monodisperse silica microspheres using Method, in a mixture of tetraethyl orthosilicate, absolute ethanol and deionized water, under room temperature (20°C-30°C), magnetic stirring, adding catalyst ammonia water (concentration: 25%-28%), reaction 6 hours, centrifuged, washed with water, and dried to obtain silica microspheres with a diameter of about 300 nm. The molar ratio of each material is: ethyl orthosilicate: ammonia water: water: absolute ethanol=1: 14: 135: 86 (TEOS: NH 3 :H 2 O:EtOH molar ratio is 1:14:135:86).
[0033] Step 2: Disperse the silica microspheres in water for ultrasonic activation, centrifuge, disperse in a large amount of absolute ethanol, add a certain amount of catalyst ammonia water (concentration is 25%-28%), ultrasonically disperse, heat in a water bath at 45°C, and magnetically Stir, and finally add tetrabutyl titanate ethanol solution, react for 2 hours, centrifuge, wash with alcohol, wash with water, and dry to ...
example 3
[0036] Step 1: Preparation of monodisperse silica microspheres using Method, in a mixture of tetraethyl orthosilicate, absolute ethanol and deionized water, under room temperature (20°C-30°C), magnetic stirring, adding catalyst ammonia water (concentration: 25%-28%), reaction 6 hours, centrifuged, washed with water, and dried to obtain silica microspheres with a diameter of about 300 nm. The molar ratio of each material is: ethyl orthosilicate: ammonia water: water: absolute ethanol=1: 14: 135: 86 (TEOS: NH 3 :H 2 O:EtOH molar ratio is 1:14:135:86).
[0037] Step 2: Disperse the silica microspheres in water for ultrasonic activation, centrifuge, disperse in a large amount of absolute ethanol, add a certain amount of catalyst ammonia water (concentration is 25%-28%), ultrasonically disperse, heat in a water bath at 45°C, and magnetically Stir, and finally add tetrabutyl titanate ethanol solution, react for 2 hours, centrifuge, wash with alcohol, wash with water, and dry to ...
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