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Composite nanometer particle and preparation method and application thereof

A composite nanoparticle and nanoparticle technology, applied in nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve the problem of single electrode optimization point, high preparation cost, and poor device efficiency lighting voltage optimization effect. large problems, to achieve the effect of improving electron mobility, simple operation, and eliminating interface defects

Active Publication Date: 2019-06-25
TCL CORPORATION
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  • Description
  • Claims
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Problems solved by technology

[0005] The object of the present invention is to provide a composite nanoparticle and its preparation method, aiming to solve the problem of single electrode optimization point, high preparation cost, efficiency of the device and lighting up in the existing electrode, especially the cathode (evaporation) preparation method. The problem of little effect of voltage optimization

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  • Composite nanometer particle and preparation method and application thereof

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preparation example Construction

[0031] Correspondingly, an embodiment of the present invention provides a method for preparing the above-mentioned composite nanoparticles, comprising the following steps:

[0032] S01. provide fullerenol and gold nanoparticles, the general formula of the fullerenol is element: C m (OH) n ;

[0033] S02. dehydration after mixing the fullererol and the silane coupling agent to prepare the fullerene modified by the silane coupling agent, the general formula of the fullerene modified by the silane coupling agent is (NH 2 -R-SiO 3 ) n C m or (SH 2 -R-SiO 3 ) n C m ;

[0034] S03. dissolving the gold nanoparticles and the fullerene modified by the silane coupling agent in an organic solvent, and under alkaline conditions, the gold nanoparticles and the fullerene are crosslinked by a silane coupling agent combine to form composite nanoparticles.

[0035] The preparation method of the composite nanoparticle provided by the embodiment of the present invention only needs to ...

Embodiment 1

[0066] A preparation method of composite nanoparticles, comprising the following steps:

[0067] S11.C 60 (OH) 36 is prepared as follows:

[0068] 10 mL (20 mmol / ml) of NaOH solution was added to the flask, and 0.5 mL (10%) of tetrabutylammonium hydroxide TBAH solution was added dropwise. With vigorous stirring, 12 mL containing 20 mg C was added dropwise 60 toluene solution, and then add dropwise 1ml (30%) of H 2 O 2 solution, and continue to stir the reaction for 2 hours. After standing, the reaction mixture was divided into two layers, the upper layer was a colorless organic phase, and the lower layer was a brown-black aqueous phase. Separation and separation, filtration to remove insoluble matter in the water phase, to obtain a brown-black solution. Methanol was added to precipitate a precipitate (soil yellow), and the methanol was removed by centrifugation; water was added to dissolve the precipitate, and then methanol was added to precipitate it, and this was repe...

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Abstract

The invention provides a composite nanometer particle which comprises gold nanometer particles and fullerene in crosslinking combination. The composite nanometer particle includes the following chemical structure unit of M@(NH-R-SiO3)nCm or M@(SH-R-SiO3)nCm, wherein @represents crosslinking combination, M represents gold nanometer particles, Cm represents fullerene, R represents an alkyl or an alkyl derivative, 28<=m<=104, 16<=n<=60, and n<m.

Description

technical field [0001] The invention belongs to the technical field of composite nanomaterials, and in particular relates to a composite nanoparticle and its preparation method and application. Background technique [0002] In the field of new display technology in the future, printing technology is expected to realize the industrial revolution of display. Display components based on quantum dot light-emitting diodes (QLED) and organic light-emitting diodes (OLED) are the subject of technical research. [0003] Printing and coating are a necessary means to realize large-area display technology. Some problems encountered when preparing large-area red, green and blue components (pixels) through printing and coating technology, such as: pixels, especially It is a blue pixel with low efficiency and high lighting voltage. At present, the analysis of these technical problems mainly takes the red, green and blue devices prepared separately by the solution method in the laboratory ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B1/02H01B1/04B82Y30/00H01L51/52H01L51/56
Inventor 程陆玲杨一行
Owner TCL CORPORATION
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