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Hydrogasification semi-coke pulping method

A technology for hydrogenation, gasification and semi-coke, which is applied in the field of coal chemical industry, can solve the problems of blockage and damage of filter 28 and induced draft fan 27, reduce the gasification efficiency of coal-water slurry, affect the gasification process of coal-water slurry, etc. The effect of pulping, improving the utilization rate of semi-coke, and ensuring continuous and stable operation

Active Publication Date: 2021-02-19
XINNENG ENERGY CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the loose and porous semi-coke texture, when it is mixed with water, it often floats on the water surface and is difficult to mix. The pulping effect is poor, and about 10% of the semi-coke by mass ratio cannot be successfully pulped. In order to ensure the pulping quality, this part is not used. The semi-coke mixed with water is generally drawn out of the pulping mixing tank 1 through the filter 28 and the induced draft fan 27. In this process, on the one hand, about 10% of the semi-coke is not effectively utilized, resulting in a waste of resources. The atmospheric environment has certain pollution; on the other hand, the filter 28 and the induced draft fan 27 are in contact with the semi-coke for a long time, and the filter 28 and the induced draft fan 27 are prone to blockage and damage, which affects the continuous and stable pulping process. Interruption will affect the progress of the coal-water slurry gasification process and reduce the efficiency of coal-water slurry gasification

Method used

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  • Hydrogasification semi-coke pulping method

Examples

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Effect test

Embodiment 1

[0020]Such asFigure 2-3 As shown, the hydrogenated semi-coke pulping device includes a pulping stirring tank 1, a Venturi mixer 2 is provided at the inlet of the pulping stirring tank 1, and a pulping agitator is provided in the pulping stirring tank 1 3. The top of the rotating shaft of the pulping agitator 3 passes through the top of the pulping agitating tank 1 and is fixedly connected with the output shaft of the pulping rotating motor 4. The top of the pulping agitating tank 1 is provided with a semi-coke treatment chamber 5, a semi-coke treatment chamber The interior of 5 is connected with the interior of the pulping mixing tank 1, the bottom of the semi-coke processing chamber 5 is connected to the top of the pulping mixing tank 1, and the top of the semi-coke processing chamber 5 is provided with an emptying pipe 6; in the semi-coke processing chamber 5 At least two arcuate trays 7 are staggered. In this embodiment, the number of trays 7 is 4, and the trays 7 are arranged ho...

Embodiment 2

[0023]The method for preparing hydrogenated semi-coke pulp by using embodiment 1 includes a start-up phase and a stable operation phase, in which:

[0024]1) Start-up stage: Add 60% of the volume of industrial fresh water into the pulp mixing tank 1, and the semi-coke is pneumatically transported to the Venturi mixer 2 to mix with the industrial fresh water transported to the Venturi mixer 2. The pressure of pneumatic conveying is 0.5MPa, the operating pressure of slurry mixing tank 1 is 0.1MPa, and the mass ratio of the semi-coke conveyed by pneumatic to the industrial fresh water introduced into the Venturi mixer 2 is 5:5, and the pre-pulping is obtained ; The pre-made slurry enters the slurry mixing tank 1 for stirring, and the stirring speed is 30r / min; during the mixing process, the industrial fresh water is introduced into the semi-coke processing chamber 5, and the semi-coke and the semi-coke are pneumatically conveyed The mass ratio of the industrial fresh water in the coke tre...

Embodiment 3

[0033]The method for preparing hydrogenated semi-coke pulp by using embodiment 1 includes a start-up phase and a stable operation phase, in which:

[0034]1) Start-up stage: Add 70% of the volume of industrial fresh water into the pulp mixing tank 1, and the semi-coke is pneumatically transported to the Venturi mixer 2 to mix with the industrial fresh water transported to the Venturi mixer 2. The pressure of pneumatic conveying is 0.6MPa, the operating pressure of slurry mixing tank 1 is 0.15MPa, the mass ratio of the semi-coke conveyed by pneumatic to the industrial fresh water introduced into the Venturi mixer 2 is 7:5, and the pre-pulping is obtained ; The pre-made pulp enters the pulp mixing tank 1 for stirring, and the stirring speed is 40r / min; during the stirring process, the industrial fresh water is introduced into the semi-coke treatment chamber 5, and the semi-coke and the semi-coke conveyed by pneumatic conveying The mass ratio of the industrial fresh water in the coke trea...

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Abstract

The invention discloses a hydrogasification semi-coke pulping method, which includes a start-up stage and a stable operation stage. The advantage of the present invention is that, through pneumatic conveying, the semi-coke is transported to the Venturi mixer to be mixed with industrial fresh water, the semi-coke is fully wetted in advance, and then the wetted semi-coke is transported to the slurry mixing tank, and the semi-coke is Coke directly enters under the liquid level of the pulping mixing tank, and is stirred with the industrial fresh water in the pulping mixing tank to make pulp, ensuring that the semi-coke is mixed into the industrial fresh water to the greatest extent, improving the utilization rate of the semi-coke and improving the pulping effect; mixing After the compressed gas with semi-coke enters the semi-coke treatment chamber, it moves upwards through the through hole of the tray. The semi-coke contacts the water film on the tray, and the semi-coke is intercepted by the water film and falls back to the pulping process with the flowing industrial fresh water. In the mixing tank, pulping is carried out, and the utilization rate of semi-coke is increased to 99%, which avoids the waste of semi-coke caused by emptying, and reduces the cost of semi-coke pulping.

Description

Technical field:[0001]The invention relates to the field of coal chemical industry, in particular to a method for preparing hydrogenated semi-coke slurry.Background technique:[0002]Hydrogenation refers to the process in which carbon-containing compounds and hydrogen react at medium temperature (700-1000°C) and high pressure (5-10MPa) to produce methane-rich crude gas, high value-added aromatic oil products and high-calorific value semi-coke. . Semi-coke is also known as low-temperature coke, gray-black, with higher volatiles than coke, loose and porous texture, and good reaction performance. It is often used as a coal-water slurry gasification raw material in the coal chemical industry.[0003]At present, the process of semi-coke used in coal water slurry gasification is roughly as follows:figure 1 As shown, the semi-coke is ground by the semi-coke mill 19, and the semi-coke with a qualified particle size is ground into the semi-coke bin 17, and the semi-coke in the semi-coke bin 17 e...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10L1/32B01F13/10
CPCC10L1/326B01F33/821
Inventor 冯浩李美喜李维张刚王凤彬王银明
Owner XINNENG ENERGY CO LTD
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