Preparation method and application of composite material Bi2O3-Co3O4 for degrading gaseous pollutants at room temperature
A technology of bi2o3-co3o4 and composite materials, applied in the direction of separation methods, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of air secondary pollution, high cost, inconvenient use, etc., and achieve easy reaction conditions, The effect of no pollution to the environment
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Embodiment 1
[0023] (1) Composite material Bi for degradation of gaseous pollutants at room temperature 2 o 3 -Co 3 o 4 preparation method
[0024] 1) Dissolve 1.94 g of cobalt nitrate hexahydrate and 1.94 g of bismuth nitrate pentahydrate in 15 mL of nitric acid, respectively, and then dilute to 50 mL respectively to obtain a solution containing bismuth and a solution containing cobalt.
[0025] 2) Mix the bismuth-containing solution and the cobalt-containing solution obtained in step 1) evenly, pour into the mixed solution of 3mL polyethylene glycol and 50mL NaOH solution with a concentration of 0.8mol / L, precipitate after stirring, and centrifuge , the obtained precipitate was washed twice with deionized water and once with ethanol, and the sample obtained after centrifugation was placed in a drying oven and dried at 100° C. for 10 h.
[0026] 3) The dried sample was calcined in a muffle furnace under air conditions at a heating rate of 5°C / min, 500°C for 2h, cooled to room temperat...
Embodiment 2
[0030] Composite Bi 2 o 3 -Co 3 o 4 Application as a catalyst in the degradation of gaseous pollutants at room temperature
[0031] (1) Degradation of formaldehyde
[0032] Method: get the composite material Bi prepared by 0.1 gram embodiment 1 2 o 3 -Co 3 o 4 Put it into a closed experimental device, inject 5 μL of 37% formaldehyde solution into the experimental device, and regularly detect the concentration of formaldehyde gas in the experimental device.
[0033] Comparative test: Inject 5 μL of 37% formaldehyde solution directly into the airtight experimental device, and regularly detect the concentration of formaldehyde gas in the experimental device.
[0034] After standing still at room temperature for 10 h, the concentration of formaldehyde gas in the experimental device was measured. Such as figure 2 as shown, figure 2 In A is the addition of composite material Bi 2 o 3 -Co 3 o 4 histogram of figure 2 In A, it can be seen that after 10 hours, the for...
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