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Mosquito-repelling and sun-proof composite functional microcapsule and preparation method thereof

A composite function and microcapsule technology, which is applied in the direction of microcapsule preparation, microsphere preparation, biochemical fiber treatment, etc., can solve the problems of unsatisfactory one-time preparation and single function of microcapsules, and achieve excellent anti-ultraviolet effect and mosquito repellent Long-lasting effect and good stability

Active Publication Date: 2019-08-20
上海驰纺材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] One of the purposes of the present invention is to provide a composite functional microcapsule for repelling mosquitoes and sunscreen and its preparation method to solve the problem that the microcapsules cannot meet the requirements of preparing multifunctional textiles due to the relatively single function of the microcapsules

Method used

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  • Mosquito-repelling and sun-proof composite functional microcapsule and preparation method thereof
  • Mosquito-repelling and sun-proof composite functional microcapsule and preparation method thereof
  • Mosquito-repelling and sun-proof composite functional microcapsule and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] (1) Preparation of acid-analyzed lignin

[0033] Weigh 0.6g of alkali lignin particles and 0.06g of sodium lauryl sulfate and disperse them in 30mL deionized water, stir them evenly with a magnetic stirrer, and adjust the pH value of the solution to about 11 with 4mol / L NaOH solution , filter to remove insoluble impurities, then use 1mol / L hydrochloric acid to adjust the pH value of the solution to 2-3, stir evenly to obtain an acid-analyzed lignin suspension, which is ready for use.

[0034] (2) Preparation of mosquito repellent sunscreen lotion

[0035] Get 7.84g of citronella oil, 0.16g of 2-hydroxy-4-methoxybenzophenone and 2.52g of isophorone diisocyanate and mix evenly, which is the oil phase. Disperse the acid-analyzed lignin suspension in step (1) into 26 mL of deionized water, which is the water phase. Slowly add the oil phase into the water phase, and emulsify for 10 min under high-speed shear at 10,000 r / min to obtain the mosquito repellent sunscreen emulsi...

Embodiment 2

[0040] (1) Preparation of acid analysis lignin

[0041] Weigh 1.2g of alkali lignin particles and 0.09g of sodium lauryl sulfate and disperse them in 30mL of deionized water, stir them evenly with a magnetic stirrer, and use 4mol / L NaOH solution to adjust the pH value of the solution to about 11 , filter to remove insoluble impurities, then use 1mol / L hydrochloric acid to adjust the pH value of the solution to 2-3, stir evenly to obtain an acid-analyzed lignin suspension, which is ready for use.

[0042] (2) Preparation of mosquito repellent sunscreen lotion

[0043] Get 7.84g of citronella oil, 0.16g of 2-hydroxy-4-methoxybenzophenone and 2.52g of isophorone diisocyanate and mix evenly, which is the oil phase. Disperse the acid-analyzed lignin suspension in step (1) into 26 mL of deionized water, which is the water phase. Slowly add the oil phase into the water phase, and emulsify for 10 min under high-speed shear at 10,000 r / min to obtain the mosquito repellent sunscreen e...

Embodiment 3

[0048] (1) Preparation of acid analysis lignin

[0049] Weigh 0.6g of alkali lignin particles and 0.06g of sodium lauryl sulfate and disperse them in 30mL deionized water, stir them evenly with a magnetic stirrer, and adjust the pH value of the solution to about 11 with 4mol / L NaOH solution , filter to remove insoluble impurities, then use 1mol / L hydrochloric acid to adjust the pH value of the solution to 2-3, stir evenly to obtain an acid-analyzed lignin suspension, which is ready for use.

[0050] (2) Preparation of mosquito repellent sunscreen lotion

[0051] Get 7.36g of citronella oil, 0.64g of 2-hydroxy-4-methoxybenzophenone and 2.52g of isophorone diisocyanate and mix evenly, which is the oil phase. Disperse the acid-analyzed lignin suspension in step (1) into 26 mL of deionized water, which is the water phase. Slowly add the oil phase into the water phase, and emulsify for 10 min under high-speed shear at 10,000 r / min to obtain the mosquito repellent sunscreen emulsi...

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Abstract

The invention relates to a mosquito-repelling and sun-proof composite functional microcapsule and a preparation method thereof. The composite functional microcapsule comprises a capsule wall supporting an ultraviolet absorption material and a capsule core wrapped in the capsule wall, wherein the ultraviolet absorption material is acidified lignin, and the capsule core is a mixture of a plant-basedmosquito repellent and an ultraviolet absorbent. The synergistic interaction between the lignin and the ultraviolet absorbent can be effectively utilized, and an excellent ultraviolet protection function can be realized on the basis of lasting mosquito repelling. The composite functional microcapsule has important application value in the fields of summer clothes, daily cosmetics and the like.

Description

technical field [0001] The invention belongs to the field of functional microcapsules, in particular to a composite functional microcapsule for repelling mosquitoes and sunscreen and a preparation method thereof. Background technique [0002] The advantages of microcapsule technology in the protection and controlled release of active substances (such as plant essential oils) have prompted it to be widely used in the textile field, such as mosquito repellent, fragrance, anti-ultraviolet and phase change microcapsules, etc. On this basis, a A series of functional textiles enhance the added value of traditional textiles. However, most of the existing microcapsules are single-functional microcapsules, and the preparation of multi-functional microcapsules is relatively rare. Taking pure cotton fabrics as an example, the acquisition of composite functions often requires the use of two or more functional finishing agents for composite finishing or multi-bath and multi-step process...

Claims

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Application Information

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IPC IPC(8): D06M23/12D06M15/01D06M13/00D06M13/152D06M15/564B01J13/14D06M101/06
CPCD06M23/12D06M15/01D06M13/00D06M13/152D06M15/564D06M16/00B01J13/14D06M2101/06D06M2200/25
Inventor 王先锋杜博超靳晓松薛东周盼红李晓宇
Owner 上海驰纺材料科技有限公司
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