MAS-LT composite microwave dielectric ceramic and preparation method thereof
A technology of microwave dielectric ceramics and ceramics, applied in the field of microwave dielectric ceramics, can solve the problems of high sintering temperature, limitation of large-scale use, large frequency temperature coefficient, etc., and achieve low sintering temperature, suitable for large-scale industrialization, and dielectric constant high effect
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[0047] The present invention also provides a method for preparing the MAS-LT composite microwave dielectric ceramic described in the above technical solution, comprising the following steps:
[0048] a) MgCO 3 、BaCO 3 、Al 2 o 3 and SiO 2 After mixing, the first grinding treatment is carried out, and then the first pre-sintering is carried out to obtain the MAS pre-sintered material;
[0049] b) put Li 2 CO 3 and TiO 2 After mixing, carry out the second grinding treatment, and then go through the second pre-sintering to obtain LT pre-sintered material;
[0050] c) After mixing the MAS calcined material and the LT calcined material, perform the third grinding treatment to obtain MAS-LT powder;
[0051] d) adding a binder to the MAS-LT powder for granulation and molding to obtain a ceramic green body; then sintering the obtained ceramic green body to obtain a MAS-LT composite microwave dielectric ceramic;
[0052] The steps a) and b) are not limited in sequence.
[0053...
Embodiment 1
[0091] (1) According to the chemical formula Mg 2 Al 4 Si 5 o 18 Weigh 50.11g MgCO 3 , 60.6g Al 2 o 3 and 89.28gSiO 2 , mixed to obtain the first mixture; the first mixture, agate balls and deionized water were wet-milled with a planetary mill for 6 hours at a mass ratio of 1:2:2, dried at 150°C, and then dried at 1000°C Pre-fire (in the air atmosphere) for 3 hours, the heating rate is 3°C / min, and cool with the furnace to obtain the MAS pre-fired material.
[0092] (2) According to Li 2 CO 3 : TiO 2 = 1:1 molar ratio weighs 96.09g Li 2 CO 3 and 103.91g TiO 2 , mixed to obtain the second mixture; the second mixture, agate balls and deionized water were wet-milled with a planetary mill for 6 hours at a mass ratio of 1:2:2, dried at 150°C, and dried at 1000°C Pre-fire (in the atmosphere) for 2 hours, the heating rate is 3°C / min, and cool with the furnace to obtain LT pre-fired material.
[0093] (3) Take by weighing 88g MAS calcined material, 12g LT calcined materi...
Embodiment 2
[0100] (1) According to the chemical formula Mg 1.92 Ba 0.08 Al 4 Si 5 o 18 Weigh 47.47g MgCO 3 , 4.63g BaCO 3 , 59.8g Al 2 o 3 and 88.1 g SiO 2 , mixed to obtain the first mixture; the first mixture, agate balls and deionized water were wet-milled with a planetary mill for 6 hours at a mass ratio of 1:2:2, dried at 150°C, and then dried at 1000°C Pre-fire (in the air atmosphere) for 3 hours, the heating rate is 3°C / min, and cool with the furnace to obtain the MAS pre-fired material.
[0101] (2) According to Li 2 CO 3 : TiO 2 = 1:1 molar ratio weighs 96.09g Li 2 CO 3 and 103.91g TiO 2 , mixed to obtain the second mixture; the second mixture, agate balls and deionized water were wet-milled with a planetary mill for 6 hours at a mass ratio of 1:2:2, dried at 150°C, and dried at 1000°C Pre-fire (in the atmosphere) for 2 hours, the heating rate is 3°C / min, and cool with the furnace to obtain LT pre-fired material.
[0102] (3) Take by weighing 88g MAS calcined mat...
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