A method of using sodium salt to strengthen the separation effect of aluminum and iron in high aluminum limonite
A technology for high-aluminum limonite and limonite, which is applied in the direction of improving process efficiency and the like, can solve the problems of fine embedded particle size and poor monomer dissociation performance, and achieves low production cost, convenient operation and simple process. Effect
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Embodiment 1
[0020] Embodiment 1: TFe content is 34.51% in the high aluminum limonite in the present embodiment, Al 2 o 3 The content is 15.72%;
[0021] A kind of method utilizing sodium salt to strengthen the separation effect of aluminum and iron of high aluminum limonite (see figure 1 ),Specific steps are as follows:
[0022] (1) Crush and finely grind high alumina limonite until the particle size is not greater than 0.074mm to obtain high alumina limonite powder, add sodium salt solution to high alumina limonite powder and mix evenly to obtain a muddy mixture; the sodium salt The solution is NaOH aqueous solution, the amount of sodium salt solution added is 12.5% of the mass of alluminite limonite powder, and the concentration of NaOH aqueous solution is 0.50g / mL;
[0023] (2) Heating the muddy mixture in step (1) at a uniform speed to a temperature of 500°C and roasting at a constant temperature for 60 minutes to obtain a roasted product, cooling the roasted product to room temp...
Embodiment 2
[0026] Embodiment 2: TFe content is 34.51% in the high aluminum limonite in the present embodiment, Al 2 o 3 The content is 15.72%;
[0027] A kind of method utilizing sodium salt to strengthen the separation effect of aluminum and iron of high aluminum limonite (see figure 1 ),Specific steps are as follows:
[0028] (1) Crush and finely grind high alumina limonite until the particle size is not greater than 0.074mm to obtain high alumina limonite powder, add sodium salt solution to high alumina limonite powder and mix evenly to obtain a muddy mixture; the sodium salt The solution is an aqueous NaOH solution, the amount of the sodium salt solution added is 16% of the mass of the high-alluminous limonite powder, and the concentration of the aqueous NaOH solution is 0.50 g / mL;
[0029] (2) Heating the muddy mixture in step (1) at a uniform speed to a temperature of 700°C and roasting at a constant temperature for 40 minutes to obtain a roasted product, cooling the roasted pro...
Embodiment 3
[0032] Embodiment 3: TFe content is 34.51% in the high aluminum limonite in the present embodiment, Al 2 o 3 The content is 15.72%;
[0033] A kind of method utilizing sodium salt to strengthen the separation effect of aluminum and iron of high aluminum limonite (see figure 1 ),Specific steps are as follows:
[0034] (1) Crush and finely grind high alumina limonite until the particle size is not greater than 0.074mm to obtain high alumina limonite powder, add sodium salt solution to high alumina limonite powder and mix evenly to obtain a muddy mixture; the sodium salt The solution is an aqueous NaOH solution, the amount of the sodium salt solution added is 15% of the mass of the high alumina limonite powder, and the concentration of the aqueous NaOH solution is 0.60 g / mL;
[0035] (2) Heating the muddy mixture in step (1) at a uniform speed to a temperature of 900°C and roasting at a constant temperature for 30 minutes to obtain a roasted product, cooling the roasted produc...
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