Algal bloom inhibitor, and preparation method and application thereof
An inhibitor and algal bloom technology, applied in the field of algal bloom inhibitor and its preparation, can solve the problems of threats to growth and survival, invasion of alien species, difficult implementation, etc. Effect
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[0032] Example 1
[0033] A method for preparing an algal bloom inhibitor provided by a preferred embodiment of the present invention, the specific steps are as follows:
[0034] Pass the shell powder through a 100-mesh sieve, and then immerse it in hydrochloric acid with a concentration of 2mol / L for 24 hours according to the volume ratio of shell powder and hydrochloric acid at 1:5, and conduct intermittent ultrasonic treatment. The continuous working time is 30s and the pulse interval is 10s; The ultrasonic frequency is 20KHz, the ultrasonic power is 200W, and it is dried at 80℃ to obtain modified shell powder;
[0035] According to the volume ratio of modified shell powder and sodium carbonate solution of 1:6, the modified shell powder was immersed in a 10mol / L sodium carbonate solution for 24 hours, and dried at 80°C to obtain treated shell powder;
[0036] Add sodium chloride to the beer fermentation waste liquid, the mass fraction of sodium chloride in the beer fermentation was...
Example Embodiment
[0039] Example 2
[0040] A method for preparing an algal bloom inhibitor provided by a preferred embodiment of the present invention, the specific steps are as follows:
[0041] Pass the shell powder through a 100-mesh sieve, and then immerse it in hydrochloric acid with a concentration of 3mol / L for 24h according to the volume ratio of shell powder and hydrochloric acid at 1:6, and perform intermittent ultrasonic treatment. The continuous working time is 60s and the pulse interval is 20s; The ultrasonic frequency is 30KHz, the ultrasonic power is 300W, and it is dried at 85℃ to obtain modified shell powder;
[0042] According to the volume ratio of modified shell powder and sodium carbonate solution of 1:67, the modified shell powder was immersed in a 12mol / L sodium carbonate solution for 24 hours and dried at 85°C to obtain treated shell powder;
[0043] Add sodium chloride to the beer fermentation waste liquid, the mass fraction of sodium chloride in the beer fermentation waste li...
Example Embodiment
[0046] Example 3
[0047] A method for preparing an algal bloom inhibitor provided by a preferred embodiment of the present invention, the specific steps are as follows:
[0048] Pass the shell powder through a 200-mesh sieve, and then immerse it in hydrochloric acid with a concentration of 3mol / L for 24h according to the volume ratio of shell powder and hydrochloric acid at 1:7, and perform intermittent ultrasonic treatment. The continuous working time is 60s and the pulse interval is 20s; The ultrasonic frequency is 40KHz, the ultrasonic power is 500W, and it is dried at 90℃ to obtain modified shell powder;
[0049] According to the volume ratio of modified shell powder and sodium carbonate solution of 1:8, the modified shell powder was immersed in a 10mol / L sodium carbonate solution for 24 hours and dried at 90°C to obtain treated shell powder;
[0050] Add sodium chloride to the beer fermentation waste liquid, the mass fraction of sodium chloride in the beer fermentation waste liq...
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