Preparation method for carbon wave-absorbing material

A technology of absorbing material and carbon, applied in textiles, papermaking, fiber processing, etc., can solve the problems of narrow absorbing frequency and deviation of absorbing performance, and achieve good wavelength absorption performance, improve efficiency, and improve wavelength absorption efficiency. Effect

Inactive Publication Date: 2019-11-08
长沙凯泽工程设计有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] The purpose of the present invention is to provide a preparation method of carbon absorbing material to s

Method used

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  • Preparation method for carbon wave-absorbing material
  • Preparation method for carbon wave-absorbing material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A preparation method of carbon absorbing material, comprising the following steps:

[0021] (1), Weigh 13.5 parts of acrylic acid, 5.2 parts of methoxypolyethylene glycol 550 monomethacrylate and 0.04 parts of 819 photoinitiator and add them to the reactor, the stirring speed is 60r / min, and the reaction temperature of the system is maintained at Stir at 40°C for 25 minutes, the product is irradiated by a 400W high-pressure mercury lamp for 2 seconds, the product is washed and dried, and the product, 18 parts of iron oxalate, 6.5 parts of cobalt oxalate and 4.5 parts of nickel oxalate are added to the reaction kettle, and the stirring speed is 50r / min, the reaction temperature was 115°C and 0.09MPa for 1.5h, the product was centrifuged and filtered, and the supernatant was heat-treated at 100°C for 0.5h, 200°C for 0.5h, 300°C for 1h, 400°C for 2h, 500 ℃ heat treatment for 2 hours, 600 ℃ heat treatment for 2 hours, 700 ℃ heat treatment for 2 hours, 800 ℃ heat treatment ...

Embodiment 2

[0026] A preparation method of carbon absorbing material, comprising the following steps:

[0027] (1), Weigh 10 parts of acrylic acid, 3 parts of methoxypolyethylene glycol 550 monomethacrylate and 0.01 part of 819 photoinitiator and add them to the reaction kettle, the stirring speed is 60r / min, and the reaction temperature of the system is maintained at Stir at 40°C for 25 minutes, the product is irradiated by a 100W high-pressure mercury lamp for 6 seconds, the product is washed and dried, and the product, 18 parts of iron oxalate, 6 parts of cobalt oxalate and 2 parts of nickel oxalate are added to the reaction kettle, and the stirring speed is 50r / min, the reaction temperature is 90°C and 0.2MPa for 1h, the product is centrifuged and filtered, the supernatant is heat-treated at 100°C for 0.5h, at 200°C for 0.5h, at 300°C for 1h, at 400°C for 2h, at 500°C Heat treatment for 2 hours, heat treatment at 600°C for 2 hours, heat treatment at 700°C for 2 hours, heat treatment ...

Embodiment 3

[0032] A preparation method of carbon absorbing material, comprising the following steps:

[0033] (1), Weigh 17 parts of acrylic acid, 8 parts of methoxypolyethylene glycol 550 monomethacrylate and 0.2 part of 819 photoinitiator and join in the reaction kettle, the stirring speed is 60r / min, and the reaction temperature of the system is maintained at Stir at 40°C for 25 minutes, the product is irradiated by a 3000W high-pressure mercury lamp for 1 second, after the product is washed and dried, the product, 18 parts of iron oxalate, 9 parts of cobalt oxalate and 5 parts of nickel oxalate are added to the reaction kettle, and the stirring speed is 50r / min, the reaction temperature is 125°C and 0.05MPa for 3h, the product is centrifuged and filtered, the supernatant is heat-treated at 100°C for 0.5h, at 200°C for 0.5h, at 300°C for 1h, at 400°C for 2h, at 500°C Heat treatment for 2 hours, heat treatment at 600°C for 2 hours, heat treatment at 700°C for 2 hours, heat treatment a...

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Abstract

The invention provides a preparation method for a carbon wave-absorbing material. The carbon wave-absorbing material is composed of a carbon matrix material, a heat conduction carbon fiber, butyl acrylate and a 819 photo-initiator, the carbon matrix material is prepared from a reaction of activated carbon sponge, mesoporous carbon, a heat conduction carbon fiber, a nano carbon material and ferrite, the heat conduction carbon fiber is prepared by reacting a carbon fiber, copper acetate, Sr-10 emulsifiers, thiourea, water, ethanol, glucose and ammonia water, and the ferrite is prepared by reacting iron oxalate, cobalt oxalate, nickel oxalate, nano copper powder, acrylic acid, methoxy polyethylene glycol 550 monomethacrylate, and the 819 photo-initiator. The carbon wave-absorbing material prepared by the method of the invention has excellent wave-absorbing properties.

Description

technical field [0001] The invention relates to the technical field of functional materials, in particular to a method for preparing a carbon wave-absorbing material. Background technique [0002] With the development of the national economy and the improvement of people's quality of life, people have gradually begun to pay attention to the effective treatment materials or methods for the electromagnetic radiation problems encountered in the living environment. However, at present, my country's electromagnetic wave absorbing materials have the defects of narrow absorbing frequency and deviation of absorbing performance. In recent years, with the continuous improvement of people's quality of life requirements, people pay special attention to materials, household appliances or equipment that are produced in the process of life and affect people's health. However, due to the electromagnetic radiation problems of many existing household appliances, Therefore, there is an urgent...

Claims

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Application Information

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IPC IPC(8): C08F292/00C08F220/18C08F2/48D06M14/36
CPCC08F2/48C08F292/00D06M14/36
Inventor 不公告发明人
Owner 长沙凯泽工程设计有限公司
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