Cured film-forming composition, alignment material, and phase difference material
A technology for curing films and compositions, applied in coatings, instruments, optics, etc., can solve problems such as the reduction of liquid crystal alignment ability, and achieve the effects of excellent solvent resistance, high sensitivity, liquid crystal alignment and excellent light transmittance
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[0204] Hereinafter, the present invention will be specifically described with reference to examples of the present invention, but the present invention should not be limited thereto.
[0205] [Abbreviated symbols used in Examples]
[0206] The meanings of the abbreviations used in the following examples are as follows.
[0207]
[0208] CIN1
[0209]
[0210] CIN2
[0211]
[0212] CIN3
[0213]
[0214] CIN4
[0215]
[0216] GMA: glycidyl methacrylate
[0217] AIBN: α,α'-Azobisisobutyronitrile
[0218] BMAA: N-Butoxymethacrylamide
[0219] HEMA: 2-Hydroxyethyl methacrylate
[0220] MMA: methyl methacrylate
[0221]
[0222] HCM: Melamine crosslinking agent represented by the following structural formula [Cymel (CYMEL) (registered trademark) 303 (manufactured by Mitsui Cytec Co., Ltd.)]
[0223]
[0224]
[0225] PTSA: p-toluenesulfonic acid monohydrate
[0226]
[0227] D-1: A compound having a hydroxyl group and an acryloyl group represented b...
reference example 1
[0240] Synthesis of CIN1
[0241] CIN1 was synthesized according to the synthesis method described in JP 2013-514449 A.
reference example 2
[0242] Synthesis of CIN2
[0243] GMA 8.3g (58.4mmol), 4-methoxycinnamic acid 20.7g (116.2mmol), dibutylhydroxytoluene 0.2g, triphenylethyl bromide 0.3g, two 80 mL of alkanes were mixed and heated at 90°C for 3 days. After the reaction is complete, the two After the alkane was distilled off under reduced pressure, 150 mL of ethyl acetate was added, the insoluble matter was separated by filtration, and 100 mL of aqueous sodium bicarbonate solution was added for washing three times to remove excess methoxycinnamic acid. Ethyl acetate was distilled off under reduced pressure to obtain CIN 216.5 g (yield: 88%) of the target substance.
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