A kind of porous microsphere foam adsorption material and preparation method thereof
A foam adsorption, porous microsphere technology, applied in chemical instruments and methods, other chemical processes, alkali metal compounds, etc., can solve the problems of environmental threats, poor circulation, poor adsorption effect, etc., to achieve the effect of strengthening mass transfer kinetics
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0020] A preparation method of a porous microsphere foam adsorption material provided by the embodiment of the present invention comprises the following steps:
[0021] Base material: under the condition of medium-speed stirring, add the cross-linking agent and catalyst and stir for 10-15 minutes to solidify the tannin solution, then add the foaming agent, and make the foam-like material after high-speed stirring. The base material is prepared by drying the material at 75-95° C. for 24-30 h.
[0022] Porous microsphere foam adsorption material: grind the base material into powder, then disperse it in a metal ion solution to prepare a mixed solution, stir the mixed solution for 25-35min and adjust its pH=4, and then adjust the pH of the mixed solution to 4. The mixed solution is stirred, suction filtered and dried to obtain a porous microsphere foam adsorption material.
[0023] Among them, tannins are a kind of natural polyphenols. In their structure, there are a large number...
Embodiment 1
[0035] A preparation method of porous microsphere foam adsorption material, comprising the following steps:
[0036] Base material: Disperse 20g of bayberry tannin in 20mL of distilled water and stir for 30min, then under the condition of 500rpm, add urotropine and p-toluenesulfonic acid and stir for 10min to solidify, then add Tween 80, stir under the condition of 1200rpm , until the volume no longer increases, then stop stirring to obtain the foamed cured tannin, and then dry the foamed cured tannin at 85°C for 24 hours to obtain the base material;
[0037] Porous microsphere foam adsorption material: 0.2546g FeCl 3 ·6H 2O was dissolved in 50 mL of distilled water to obtain a metal ion solution, the base material was ground into powder, 1 g of the powdery base material was dispersed in the metal ion solution to obtain a mixed solution, and the mixed solution was stirred for 30 min and adjusted to pH=4, Then, the mixed solution was stirred for 3 hours, filtered with suction...
Embodiment 2
[0039] A preparation method of porous microsphere foam adsorption material, comprising the following steps:
[0040] Base material: Disperse 20g of bayberry tannin in 24mL of distilled water and stir for 25min, then under the condition of 400rpm, add urotropine and p-toluenesulfonic acid and stir for 15min to solidify, then add Tween 80, stir under the condition of 1200rpm , until the volume no longer increases, stop stirring to obtain foamy cured tannins, and then dry the foamy cured tannins at 75°C for 22 hours to obtain the base material;
[0041] Porous microsphere foam adsorption material: 0.2546g FeCl 3 ·6H 2 O was dissolved in 40 mL of distilled water to prepare a metal ion solution, the base material was ground into powder, 1 g of the powdery base material was dispersed in the metal ion solution to obtain a mixed solution, and the mixed solution was stirred for 25 min and adjusted to pH=4, Then, the mixed solution was stirred for 3 hours, filtered with suction, and d...
PUM
| Property | Measurement | Unit |
|---|---|---|
| clearance rate | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More