A kind of matting agent and its preparation method, the underfill glue containing it and its application
A technology of bottom filling glue and matting agent, applied in the direction of chemical instruments and methods, adhesives, adhesive types, etc., can solve the problem of reducing the contrast and clarity of LED display screens, increasing the surface reflectivity of the screen body, and not suitable for LED display screens and other problems, to achieve the effect of fast curing, good connection reliability, and reduced gloss
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preparation example 1
[0072] A matting agent is a methyl silicone resin modified silicon dioxide, and the preparation method is as follows:
[0073] (a) Dissolve 50g of silane coupling agent γ-glycidyl etheroxypropyltrimethoxysilane in 950g of ethanol to prepare a 5wt% solution, then add acetic acid to the solution and adjust the pH value to 4-5 ;
[0074] (b) Add 200g of 0.6μm silicon dioxide powder and 100g of 2μm methyl silicone resin powder to the above solution in sequence, and disperse at high speed;
[0075] (c) Finally, the above product was filtered, washed, dried and pulverized to obtain 300 g of a matting agent.
preparation example 2-4
[0077] The only difference with Preparation Example 1 is that in this preparation example, the total mass of silicon dioxide and methyl silicone resin is kept constant at 300g, and the mass ratio of silicon dioxide and methyl silicone resin is 1:1 (preparation example 2), 1:2 (preparation example 3), 1:5 (preparation example 4).
preparation example 5-6
[0079] The only difference with Preparation Example 1 is that in step (a) of this Preparation Example, the total mass of the solution is kept constant at 1000 g, and the amount of silane coupling agent added is 10 g (Preparation Example 5), 100 g (Preparation Example 6) .
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