Preparation method of rare earth high-temperature carbon paste for microcrystalline glass plate
A high-temperature carbon and glass plate technology, used in equipment for manufacturing conductive/semiconductor layers, cable/conductor manufacturing, electrical components, etc. It is easy to corrode glass and other problems, so as to ensure the appearance and use effect, high use temperature and excellent firing characteristics.
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[0034] The invention provides a technical solution: a preparation method of rare earth high temperature carbon paste for glass-ceramic plates, the composition of the rare earth high temperature carbon paste includes a combination of solid phase components and organic binders, and the solid phase components and organic The ratio of the solvent is (60-80): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, and the high-temperature lead-free glass powder is composed of lead-free glass and rare earth materials, so The ratio of the high-temperature lead-free rare earth glass to graphite carbon powder is (60-80): (20-40), and the particle diameters are all less than 1цm.
[0035] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, comprising the steps of:
[0036] A. First mix various raw materials of high-temperature lead-free glass powder, then melt in a heating furnace at 1350°C, an...
Embodiment 1
[0040] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, the composition of the rare-earth high-temperature carbon paste includes a solid phase component and an organic binder combination, and the ratio of the solid phase component to the organic solvent is (60-80 ): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, the high-temperature lead-free glass powder includes lead-free glass and rare earth materials, and the high-temperature lead-free rare-earth glass and graphite The ratio of carbon powder is (60~80):(20~40), and the particle size is less than 1μm. The various raw materials and weight ratios of the high-temperature lead-free glass powder are:
[0041] Bi 2 o 3 : 20~40%
[0042] B 2 o 3 : 20~42%
[0043] SiO 2 : 10~15%
[0044] La 2 o 3 : 5~9%
[0045] TiO 2 : 1%~6%
[0046] Al 2 o 3 : 6%~16%
[0047] ZnO: 12% to 15%
[0048] MgO: 0.5% to 4%
[0049] ...
Embodiment 2
[0055] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, the composition of the rare-earth high-temperature carbon paste includes a solid phase component and an organic binder combination, and the ratio of the solid phase component to the organic solvent is (60-80 ): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, the high-temperature lead-free glass powder includes lead-free glass and rare earth materials, and the high-temperature lead-free rare-earth glass and graphite The ratio of carbon powder is (60~80):(20~40), and the particle size is less than 1μm. The various raw materials and weight ratios of the high-temperature lead-free glass powder are:
[0056] Bi 2 o 3 : 20~40%
[0057] B 2 o 3 : 20~42%
[0058] SiO 2 : 10~15%
[0059] La 2 o 3 : 5~9%
[0060] TiO 2 : 1%~6%
[0061] Al 2 o 3 : 6%~16%
[0062] ZnO: 12% to 15%
[0063] MgO: 0.5% to 4%
[0064] ...
PUM
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