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Preparation method of rare earth high-temperature carbon paste for microcrystalline glass plate

A high-temperature carbon and glass plate technology, used in equipment for manufacturing conductive/semiconductor layers, cable/conductor manufacturing, electrical components, etc. It is easy to corrode glass and other problems, so as to ensure the appearance and use effect, high use temperature and excellent firing characteristics.

Inactive Publication Date: 2020-01-14
TAIYANG ELECTRONICS DONGGUAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide a method for preparing rare earth high-temperature carbon paste for glass-ceramics, which has the advantage of high practicability, and solves the problem that the existing carbon paste used as thick film resistors has a relatively low temperature and cannot Applied to glass-ceramic plates, the slurry above 200°C is easy to corrode the glass, which affects the appearance and use effect of the glass

Method used

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preparation example Construction

[0034] The invention provides a technical solution: a preparation method of rare earth high temperature carbon paste for glass-ceramic plates, the composition of the rare earth high temperature carbon paste includes a combination of solid phase components and organic binders, and the solid phase components and organic The ratio of the solvent is (60-80): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, and the high-temperature lead-free glass powder is composed of lead-free glass and rare earth materials, so The ratio of the high-temperature lead-free rare earth glass to graphite carbon powder is (60-80): (20-40), and the particle diameters are all less than 1цm.

[0035] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, comprising the steps of:

[0036] A. First mix various raw materials of high-temperature lead-free glass powder, then melt in a heating furnace at 1350°C, an...

Embodiment 1

[0040] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, the composition of the rare-earth high-temperature carbon paste includes a solid phase component and an organic binder combination, and the ratio of the solid phase component to the organic solvent is (60-80 ): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, the high-temperature lead-free glass powder includes lead-free glass and rare earth materials, and the high-temperature lead-free rare-earth glass and graphite The ratio of carbon powder is (60~80):(20~40), and the particle size is less than 1μm. The various raw materials and weight ratios of the high-temperature lead-free glass powder are:

[0041] Bi 2 o 3 : 20~40%

[0042] B 2 o 3 : 20~42%

[0043] SiO 2 : 10~15%

[0044] La 2 o 3 : 5~9%

[0045] TiO 2 : 1%~6%

[0046] Al 2 o 3 : 6%~16%

[0047] ZnO: 12% to 15%

[0048] MgO: 0.5% to 4%

[0049] ...

Embodiment 2

[0055] A method for preparing rare earth high-temperature carbon paste for glass-ceramic plates, the composition of the rare-earth high-temperature carbon paste includes a solid phase component and an organic binder combination, and the ratio of the solid phase component to the organic solvent is (60-80 ): (20-40), the solid phase components include graphite carbon powder and high-temperature lead-free glass powder, the high-temperature lead-free glass powder includes lead-free glass and rare earth materials, and the high-temperature lead-free rare-earth glass and graphite The ratio of carbon powder is (60~80):(20~40), and the particle size is less than 1μm. The various raw materials and weight ratios of the high-temperature lead-free glass powder are:

[0056] Bi 2 o 3 : 20~40%

[0057] B 2 o 3 : 20~42%

[0058] SiO 2 : 10~15%

[0059] La 2 o 3 : 5~9%

[0060] TiO 2 : 1%~6%

[0061] Al 2 o 3 : 6%~16%

[0062] ZnO: 12% to 15%

[0063] MgO: 0.5% to 4%

[0064] ...

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Abstract

The invention discloses a preparation method of rare earth high-temperature carbon paste for a microcrystalline glass plate. The rare earth high-temperature carbon paste comprises combination of a solid-phase component and an organic binder, wherein the ratio of the solid-phase component to the organic binder is (60-80):(20-40), wherein the solid-phase component comprises graphite carbon powder and high-temperature lead-free glass powder, high-temperature lead-free glass powder comprises lead-free glass neutralized rare earth materials, the ratio of the high-temperature lead-free rare earth glass to the graphite carbon powder is (60-80):(20-40), the particle sizes of the high-temperature lead-free rare earth glass and the graphite carbon powder are both smaller than 1 [mu]m, and the viscosity of the rare earth high-temperature carbon paste in various proportions is 100-200 mPas. Compared with traditional carbon paste, the rare earth high-temperature carbon paste has the advantages of being high in temperature, environmentally friendly, high in use temperature, adjustable in sheet resistance and excellent in firing characteristic, can be directly smeared on the surface of a microcrystalline glass plate, does not corrode the microcrystalline glass plate in a high-temperature state, and greatly guarantees the attractiveness and the use effect of the glass.

Description

technical field [0001] The invention relates to the technical field of rare-earth high-temperature carbon paste, in particular to a preparation method of rare-earth high-temperature carbon paste for a glass-ceramic plate. Background technique [0002] In the field of electric heating, the new type of heating element requires small volume, high power, large surface heat load, low enthusiasm, high thermal efficiency, low power consumption, fast heat start, uniform temperature field, and no heating. Electromagnetic pollution, green, environmental protection, safe and reliable. Electronic paste is the basic material for the manufacture of thick film components. It is a paste made of solid powder and organic solvents that are mixed uniformly by three-roll rolling. In the field of thick film circuit technology, traditional substrates include ceramic substrates and metals, both of which have their limitations. At present, the carbon paste used at home and abroad as a thick film r...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B13/00C03C17/00
CPCC03C17/009H01B13/0026
Inventor 刘应华陈凯罗国强谢化东
Owner TAIYANG ELECTRONICS DONGGUAN
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