Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Synthesis method of non-corrosive acrylate rubber

A technology of acrylate and synthesis method, which is applied in the field of acrylate rubber preparation, and can solve the problems of slow vulcanization, poor processability of rollers, shortening the service life of processing molds, etc.

Inactive Publication Date: 2021-05-18
无锡市诺邦橡塑有限公司
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In view of the above situation, in order to overcome the defects of the prior art, the present invention provides a synthetic method of non-corrosive acrylic rubber, which effectively solves some shortcomings of the existing acrylic rubber: strong corrosion to the processing mold The service life of the processing mold is shortened; the processability of the roller is poor, and the phenomenon of sticking the roller is more serious; the vulcanization is slow, and secondary vulcanization is required; the problem of poor water resistance and low temperature resistance

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Synthesis method of non-corrosive acrylate rubber

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0024] see figure 1 , the synthetic method of a kind of non-corrosion type acrylate rubber of the present invention, comprises the following steps:

[0025] S1: Preparation materials: prepare 10-35 parts of ethyl acrylate rubber, 15-25 parts of ethyl acrylate rubber, 20-45 parts of diene rubber, 5-12 parts of allyl glycidyl ether solution, and glycidyl methacrylate 4-8 parts of solution, 2-5 parts of reinforcing agent, 3-10 parts of accelerator, 2-8 parts of anti-aging agent, 1-3 parts of anti-scorch agent, 5-13 parts of lubricant, 4-8 parts of plasticizer , 4-6 parts of antioxidant, 5-6 parts of flame retardant, 4-6 parts of compatibilizer, 4-12 parts of emulsifier, 4-10 parts of initiator, 3-5 parts of molecular weight regulator and 5-5 parts of coagulant 20 backups;

[0026] S2: Primary mixing: 10-35 parts of ethyl acrylate rubber, 15-25 parts of ethyl acrylate rubber, 20-45 parts of diene rubber, 2-5 parts of reinforcing agent, 3-10 parts of accelerator and compatibilize...

Embodiment 1

[0032] A kind of synthetic method of non-corrosion type acrylate rubber, comprises the following steps:

[0033] S1: Prepare materials: Prepare 10 parts of ethyl acrylate rubber, 15 parts of ethyl acrylate rubber, 20 parts of diene rubber, 5 parts of allyl glycidyl ether solution, 4 parts of glycidyl methacrylate solution, and 2 reinforcing agents 3 parts, 3 parts of accelerator, 2 parts of anti-aging agent, 1 part of anti-scorch agent, 5 parts of lubricant, 4 parts of plasticizer, 4 parts of antioxidant, 5 parts of flame retardant, 4 parts of compatibilizer, 4 parts of emulsifier , 4 parts of initiator, 3 parts of molecular weight regulator and 5 parts of coagulant for standby;

[0034] S2: One-time mixing: put 10 parts of ethyl acrylate rubber, 15 parts of ethyl acrylate rubber, 20 parts of diene rubber, 2 parts of reinforcing agent, 3 parts of accelerator and 4 parts of compatibilizer into the reactor and stir and mix. The temperature in the kettle is set at 35°C, the mixi...

Embodiment 2

[0040] A kind of synthetic method of non-corrosion type acrylate rubber, comprises the following steps:

[0041] S1: Prepare materials: Prepare 35 parts of ethyl acrylate rubber, 25 parts of ethyl acrylate rubber, 45 parts of diene rubber, 12 parts of allyl glycidyl ether solution, 8 parts of glycidyl methacrylate solution, and 5 parts of reinforcing agent 10 parts, accelerator 10 parts, anti-aging agent 8 parts, anti-scorch agent 3 parts, lubricant 13 parts, plasticizer 8 parts, antioxidant 6 parts, flame retardant 6 parts, compatibilizer 6 parts, emulsifier 12 parts , 10 parts of initiator, 5 parts of molecular weight regulator and 20 parts of coagulant for standby;

[0042] S2: One-time mixing: put 35 parts of ethyl acrylate rubber, 25 parts of ethyl acrylate rubber, 45 parts of diene rubber, 5 parts of reinforcing agent, 10 parts of accelerator and 6 parts of compatibilizer into the reactor and stir and mix. The temperature in the kettle is set at 45°C, the mixing reactio...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to the technical field of preparation of acrylate rubber, and discloses a synthesis method of non-corrosive acrylate rubber. The synthesis method of the non-corrosive acrylate rubber comprises the following steps: S1, preparation of materials; S2, primary mixing; S3, secondary mixing; S4, melting and mixing; and S5, vulcanization and shaping. Compared with a traditional TCY vulcanization system, the method of the invention has the advantages that a vulcanization speed is higher, a mold cannot be corroded, and the service life of the mold is effectively prolonged; and since methyl acrylate rubber, ethyl acrylate rubber and diene rubber serve as raw materials, and the diene rubber is high in stability, so the heat resistance, the tensile strength, the hardness and the oil resistance of the acrylate rubber can be effectively improved, the phenomenon of roller sticking caused by excessive softness and excessive adhesion during rubber mixing can be avoided, the low temperature resistance of the acrylate rubber is enhanced to a certain extent, practical performance is improved, a production process is simpler, and production efficiency is effectively improved.

Description

technical field [0001] The invention belongs to the technical field of acrylate rubber preparation, in particular to a method for synthesizing non-corrosive acrylate rubber. Background technique [0002] Acrylate rubber is an elastomer obtained by copolymerization of acrylate as the main monomer. Its main chain is a saturated carbon chain and its side groups are polar ester groups. Due to the special structure endows it with many excellent characteristics, such as: heat resistance, aging resistance, oil resistance, ozone resistance, UV resistance, etc., its mechanical properties and processing properties are superior to fluororubber and silicone rubber, and its heat resistance, aging resistance and oil resistance Superior to nitrile rubber. [0003] The existing acrylate rubber also has some disadvantages: it is highly corrosive to the processing mold, which shortens the service life of the processing mold; the processability of the roller is poor, and the phenomenon of sti...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C08L9/00C08L33/04C08K5/1515
CPCC08L9/00C08L2205/025C08L2205/03C08L2201/08C08L2201/02C08L33/04C08K5/1515
Inventor 王达兵王俊杰
Owner 无锡市诺邦橡塑有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products