Building insulation coil containing phase change material and preparation method thereof
A technology of phase change materials and building insulation, applied in building insulation materials, roofs using flexible materials, buildings, etc., can solve the problems of poor air permeability, unfavorable transportation and construction of buildings with specific structures, and achieve small footprint, Easy to store, guaranteed dry effect
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Embodiment 1
[0042] 1. Preparation of building insulation coils containing phase change materials:
[0043] (1) Preparation of phase change material: Add 10gMMA and 3g initiator BPO into a 250ml three-neck flask for heating in a water bath, and prepolymerize at 65°C for 30min, then add 10gAA for prepolymerization for 30min, then add 60g No. 30 paraffin and 2g crosslinking agent Add DVB into the three-necked flask of pre-polymerization solution, mix and react for 10 minutes, and use it as the oil phase; pour 500g of water preheated at the same temperature and 0.4g of dispersant triethanolamine as the continuous phase into a constant temperature water bath cup, open Shear emulsifier, and put the oil phase into the water phase for shear dispersion. After 3 minutes, transfer the mixed solution into a three-necked flask, and raise the temperature to 75°C for reaction. The reaction time is 5h, and the prepared microcapsule mixture is Filter, wash repeatedly with distilled water, and finally dry ...
Embodiment 2
[0051] 1. Preparation of building insulation coils containing phase change materials:
[0052] (1) Preparation of phase change material: Add 10gMMA and 3g initiator BPO into a 250ml three-neck flask for heating in a water bath, and prepolymerize at 65°C for 30min, then add 10gAA for prepolymerization for 30min, then add 60g No. 30 paraffin and 2g crosslinking agent Add DVB into the three-necked flask of pre-polymerization solution, mix and react for 10 minutes, and use it as the oil phase; pour 500g of water preheated at the same temperature and 0.4g of dispersant triethanolamine as the continuous phase into a constant temperature water bath cup, open Shear emulsifier, and put the oil phase into the water phase for shear dispersion. After 3 minutes, transfer the mixed solution into a three-necked flask, and raise the temperature to 75°C for reaction. The reaction time is 5h, and the prepared microcapsule mixture is Filter, wash repeatedly with distilled water, and finally dry ...
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