Al4SiC4 ternary non-oxide converter slag-stopping sliding plate and preparation method thereof
A converter slag blocking and non-oxide technology, which is applied in the field of adding Al4SiC4 ternary non-oxide converter slag blocking sliding bricks and its preparation, can solve the problems of low temperature strength reduction, poor thermal shock stability, etc., and achieves increased strength, improved High temperature strength, effect of improving oxidation resistance
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Embodiment 1
[0047] The addition of Al in this embodiment 4 SiC 4The preparation method of the ternary non-oxide converter slag retaining slide brick comprises the following steps:
[0048] (1) Fine powder premixing: the platy corundum fine powder, Al 4 SiC 4 Fine powder, active α-Al 2 o 3 Micropowder, carbon black, metal Al powder, and composite antioxidant are premixed in a V-shaped mixer for 60 minutes, and the premixed fine powder is placed in a dry kang room at 60°C for 3 days;
[0049] (2) Particle material batching: 2.3-1mm tabular alumina particles, 1-0.5mm tabular corundum particles and 0.5-0.045mm tabular corundum particles are batched according to the weight percentage by the automatic batching system;
[0050] (3) Mixing and milling: Dry mix the granules in step (2) in an inclined high-speed mixer for 3 minutes, then add 4% composite liquid resin binder (first add silicone resin, then add phenolic resin) and wet mix 6 minutes, then add the pre-mixed fine powder in (1) ste...
Embodiment 2
[0059] The composition and weight percentage of the converter slag blocking slide described in this embodiment are: 28% of plate-shaped corundum particles with a particle diameter of 2.3-1mm, 17% of plate-shaped corundum particles with a particle diameter of 1-0.5mm, and a particle diameter of 0.5-0.045mm plate-shaped corundum particles 19%, 0-0.045mm plate-shaped corundum fine powder 14%, active α-Al 2 o 3 Micropowder 6.5%, Al 4 SiC 4 5% fine powder, 2.5% carbon black, 4% active metal aluminum powder, 4% composite antioxidant, the total percentage is 100%; plus 4.5% liquid resin binder.
Embodiment 3
[0061] The composition and weight percentage of the converter slag blocking slide described in this embodiment are: 31% of plate-shaped corundum particles with a particle diameter of 2.3-1mm, 15% of plate-shaped corundum particles with a particle diameter of 1-0.5mm, and a particle diameter of 0.5-0.045mm plate-shaped corundum particles 18%, 0-0.045mm plate-shaped corundum fine powder 15%, active α-Al 2 o 3 Micropowder 5%, Al 4 SiC 4 4% of fine powder, 3% of carbon black, 5% of active metal aluminum powder, 4% of composite antioxidant, the total percentage is 100%, and 5% of liquid resin binder is added.
[0062] The addition of Al described in Table 1 Examples 1 to 3 4 SiC 4 Physical and chemical properties of ternary non-oxide converter slag retaining slide
[0063]
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