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A special calcium-based powder modification device and modification method for adhesives

A calcium-based powder and adhesive technology, which is applied in the field of special calcium-based powder modification devices for adhesives, can solve the problems of poor uniformity of the powder surface modifier, and achieves the advantages of avoiding excessive storage time, stable quality, and improved technology. simple effect

Active Publication Date: 2021-06-18
SICHUAN YIXIN NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to overcome the shortcoming that in the prior art, in the dry method modification, when modifying the calcium carbonate powder, modifying agent is added in the kneader, so that the uniformity of the powder surface modifying agent is not good , to provide a calcium-based powder modification device for adhesives, through which the modifier can make the powder more uniform during modification and improve the activation degree of the powder; at the same time, it also provides a special calcium-based powder for adhesives Powder modification method for modifying powder

Method used

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  • A special calcium-based powder modification device and modification method for adhesives
  • A special calcium-based powder modification device and modification method for adhesives

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Embodiment 1

[0026] This implementation discloses a special calcium-based powder modification device for adhesives, including a grinder 1, a kneader 2 connected to the grinder 1, and a mixing device 3 arranged between the grinder 1 and the kneader 2. The mixing The device 3 includes a mixing chamber 4, a modifying agent nozzle 5, a hot high-pressure air nozzle 6, and a powder nozzle 7. The powder nozzle 7 is located at the top of the mixing chamber 4 and one end extends into the mixing chamber 4, and the other end passes through the A high-speed airflow disperser 8 is connected with the grinder 1, the hot high-pressure jet pipe 6 is located directly below the powder jet pipe 7, the nozzle of the powder jet pipe 7 is opposite to the hot high-pressure jet pipe 6 nozzle, and the modified One end of the agent spray pipe 5 extends into 6 positions of the hot high-pressure air spray pipe, and the nozzle of the modifier nozzle 5 is 2-3 cm higher than the 6 nozzles of the hot high-pressure air spra...

Embodiment 2

[0035] This embodiment discloses a calcium-based powder modification method for adhesives as follows, including using the modification device described in Embodiment 1;

[0036] Specifically include the following steps,

[0037] S1: Put the pulverized and homogenized calcium carbonate into the grinder 1 for grinding;

[0038] S2: The ground powder enters the mixing chamber 4 to be mixed with the modifier;

[0039] S3: The mixed powder enters the kneader 2 for kneading modification.

[0040] Among them, in S1, the grinder 1 grinds calcium carbonate to 2900 mesh, and in S2, the hot high-pressure gas ejected from the hot high-pressure gas injection pipe 6 in the mixing chamber 4 is T=95°C, P=2.5Mpa.

[0041] Wherein, the modifying agent in S2 includes 10 parts of stearic acid, 5 parts of silane coupling agent, 4 parts of titanate coupling agent, and 1 part of aluminate coupling agent, and the modifier is mixed before use. Mixed preparations.

[0042]Among them, in S3, after t...

Embodiment 3

[0046] This embodiment is further optimized on the basis of Embodiment 2, wherein, in S1, the grinding machine 1 grinds calcium carbonate to 2800 mesh, and in S2, the hot high-pressure gas ejected from the hot high-pressure gas injection pipe 6 in the mixing chamber 4 T=90°C, P=2Mpa.

[0047] Wherein, the modifying agent in S2 includes 15 parts of stearic acid, 6 parts of silane coupling agent, 5 parts of titanate coupling agent, and 3 parts of aluminate coupling agent.

[0048] Example 3

[0049] This embodiment is further optimized on the basis of Embodiment 2, wherein, in S1, the grinding machine 1 grinds calcium carbonate to 3000 meshes, and in S2, the hot high-pressure gas ejected from the hot high-pressure gas injection pipe 6 in the mixing chamber 4 T=100°C, P=3Mpa.

[0050] Wherein, the modifying agent in S2 includes 20 parts of stearic acid, 8 parts of silane coupling agent, 6 parts of titanate coupling agent, and 5 parts of aluminate coupling agent.

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Abstract

The invention discloses a special calcium-based powder modifying device for adhesive, which comprises a grinder and a kneader connected with the grinder, and also includes a mixing device arranged between the grinder and the kneader, the mixing device includes a mixing chamber, modifier nozzle, hot high-pressure gas nozzle, powder nozzle, the powder nozzle is located in the upper part of the mixing chamber and one end extends into the mixing chamber; the invention also discloses a special calcium-based powder modified The method includes a modification step using a special calcium-based powder modification device for adhesives. The present invention can make the modifier on the surface of the powder more uniform by mixing the modifier and the powder before kneading, and at the same time, ensure that the powder The adhesion rate of the body surface modifier, the powder is fully attached to the modifier and then enters the kneader for kneading modification to ensure the quality of the powder and can effectively improve the activation degree of the powder. It has the advantages of simple process, improved The advantage of the activation degree of powder after curing is greater than 90%.

Description

technical field [0001] The invention relates to a special calcium-based powder modification device for adhesives, and also relates to a modification method, which belongs to the technical field of calcium carbonate modification. Background technique [0002] Calcium carbonate has the advantages of low price, non-irritating, non-toxic, good color and high whiteness. In the adhesive industry, calcium carbonate is one of the most widely used inorganic fillers. [0003] At present, the output and market share of heavy calcium carbonate in my country are far greater than that of light calcium carbonate, but the most advanced grinding technology in the world can only make the particle size of heavy calcium carbonate reach about 1 μm. This scale of heavy calcium carbonate filled in the resin matrix can only play a strengthening role, and cannot achieve the effect of toughening and functionalization. Therefore, in order to further expand the application fields and prospects of heav...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09C1/02C09C3/04C09C3/08C09C3/12C09J11/04
CPCC01P2006/19C09C1/021C09C3/006C09C3/04C09C3/08C09C3/12C09J11/04
Inventor 彭贵明徐霞彭建蓉陈华平
Owner SICHUAN YIXIN NEW MATERIAL CO LTD
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