Cement early strength agent composition and preparation method thereof
A technology of early strength agent and composition, applied in the field of cement early strength agent, can solve the problems such as difficulty in controlling the dosage of triethanolamine type early strength agent, reduction of concrete impermeability and corrosion resistance, reduction of concrete workability and durability, etc. , to reduce maintenance energy consumption, speed up mold turnover, and improve ultra-early strength.
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Embodiment 1
[0034] Weigh 38.25g of calcium chloride and 50.15g of water to configure calcium chloride aqueous solution, weigh 43.74g of potassium silicate and 44.26g of water to configure potassium silicate solution, weigh 23.80g of dispersant and 158.2g of water to configure composite dispersant aqueous solution. The composite dispersant solution was introduced into a three-necked flask, the temperature was set at 15°C, and the dispersant solution was stirred evenly. Under the condition of keeping stirring, the calcium chloride aqueous solution and the potassium silicate aqueous solution are added dropwise at the same time, and the dropping rate is adjusted so that the dropping time is controlled at about 1 hour. Continue stirring for 1 h after the dropwise addition, and then slowly cool down to room temperature to obtain the early strengthening agent HA-1.
Embodiment 2
[0036] Weigh 54.85g of calcium nitrate and 55.29g of water to configure calcium nitrate aqueous solution, weigh 53.74g of water glass and 44.26g of water to configure water glass solution, weigh 22.72g of dispersant and 141.5g of water to configure composite dispersant aqueous solution. The composite dispersant solution was introduced into a three-necked flask, the temperature was set at 15°C, and the dispersant solution was stirred evenly. Under the condition of keeping stirring, the calcium chloride aqueous solution and the potassium silicate aqueous solution are added dropwise at the same time, and the dropping rate is adjusted so that the dropping time is controlled at about 2 hours. Continue to stir for 4 hours after the dropwise addition, and then slowly cool down to room temperature to obtain the early strengthening agent HA-2.
Embodiment 3
[0038] Weigh 44.85g of calcium formate and 53.57g of water to configure calcium formate aqueous solution, weigh 48.36g of potassium metasilicate and 43.78g of water to configure potassium metasilicate solution, weigh 24.18g of dispersant and 133.5g of water to configure composite dispersant aqueous solution. The composite dispersant solution was introduced into a three-necked flask, the temperature was set at 15°C, and the dispersant solution was stirred evenly. Under the condition of keeping stirring, the calcium chloride aqueous solution and the potassium silicate aqueous solution are added dropwise at the same time, and the dropping rate is adjusted so that the dropping time is controlled at about 7 hours. Continue to stir for 3 hours after the dropwise addition, and then slowly cool down to room temperature to obtain the early strengthening agent HA-3.
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