Waterproof foam with buffering performance and hydrophobicity
A waterproof foam, hydrophobic technology, applied in the coating and other directions, can solve the problems of uneven thickness control, poor buffering ability, easy to absorb water, etc., achieve controllable thickness range, improve high temperature resistance and waterproof and hydrophobic, improve The effect of thickness uniformity
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Embodiment A
[0058] The method of adding hollow microspheres is:
[0059] (1) Dissolve the elastomer resin A with a dissolving solvent, and control the solution viscosity at 6000-8000mpa.s;
[0060] (2) Add the hollow microspheres to the above-mentioned elastomer resin A liquid, disperse at 500 rpm for 30 minutes, stir evenly, then stir and disperse at 1000 rpm for 30 minutes to obtain a pretreatment solution;
[0061] (3) Add the pretreatment solution into a closed reaction kettle, first pass nitrogen, then gradually heat up to 80 ° C, dropwise add 5% isocyanate dimer of the hollow microsphere mass, and T12 catalyst of 0.1% of the total component mass , constant temperature reaction for 2h; the material of hollow microspheres is acrylic material;
[0062] (4) At a constant temperature of 80°C, gradually add the hydrolyzed hexadecane silane coupling agent as a long-chain alkane type compound until the NCO content in the system drops to 0.1%, to obtain hollow microspheres and elastomer res...
Embodiment B
[0075] mixing elastomer resin A, elastomer resin B, hollow microspheres, silane coupling agent, flame retardant, antioxidant and dissolving solvent;
[0076] The neutral body resin A is selected from the block polymer of styrene-butadiene and the block polymer of styrene-isoprene; the elastomer resin B is acrylic resin to styrene-butadiene and its block Modified polymers; hollow microspheres are treated as in Example B1 and Example B2; the silane coupling agent is selected from vinyl silane coupling agents; the flame retardant is a phosphorus-based halogen-free flame retardant and a nitrogen-based The combination of halogen-free flame retardants; the antioxidant is a combination of hindered phenolic antioxidant and phosphite antioxidant, the two are mixed at a ratio of 1:1; the dissolving solvent is a mixed solvent of cyclohexane and hydrogenated toluene.
[0077] Wherein, embodiment B1: the method of adding hollow microspheres is:
[0078] (1) Dissolve the elastomer resin A ...
Embodiment B2
[0081] Embodiment B2: the method of adding hollow microspheres is:
[0082] (1) Dissolve the elastomer resin A with a dissolving solvent, and control the solution viscosity at 6000-8000mpa.s;
[0083] (2) Add the hollow microspheres to the above-mentioned elastomer resin A liquid, disperse at 500 rpm for 30 minutes, stir evenly, then stir and disperse at 1000 rpm for 30 minutes to obtain a pretreatment solution;
[0084] (3) Add the pretreatment solution into a closed reaction kettle, first pass nitrogen, then gradually heat up to 80 ° C, dropwise add 5% isocyanate dimer of the hollow microsphere mass, and T12 catalyst of 0.1% of the total component mass , constant temperature reaction for 2h; the material of hollow microspheres is acrylic material;
[0085] (4) At a constant temperature of 80°C, gradually add the hydrolyzed hexadecane silane coupling agent as a long-chain alkane type compound until the NCO content in the system drops to 0.1%, to obtain hollow microspheres an...
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