Aging-resistant colored pervious concrete and preparation method thereof
A permeable concrete and anti-aging technology, which is applied in the field of building materials, can solve the problems of colored concrete that is easy to age and fade, and achieve the effects of adjustable performance, improved tensile strength, and improved durability
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Embodiment 1
[0036](1) Dissolve 0.35kg of cellulose in a solution of 6.5kg of sodium hydroxide and 32kg of water to make a cellulose solution, then heat to 60°C and add 8kg of β-cyclodextrin, stir until completely dissolved, then add 4kg of silicon Acetate ethyl ester, then slowly drop into 0.12kg cyclohydrochloropropane and continue to mix and stir to obtain cellulose-modified β-cyclodextrin hydrogel;
[0037] (2) Phosphoric acid was added dropwise to the cellulose-modified β-cyclodextrin hydrogel to adjust the pH value to 2, so that tetraethyl orthosilicate was hydrolyzed, and in the interior of the cellulose-modified β-cyclodextrin hydrogel Form silica hydrogel;
[0038] (3) Add silica hydrogel to water, soak and age for 3 days, after soaking, the hydrogel becomes translucent, and a translucent hydrogel is obtained;
[0039] (4) Freeze-dry the translucent hydrogel at -20°C for 25 hours, and freeze-dry to prepare a silica-complexed β-cyclodextrin aerogel, which is pulverized and used fo...
Embodiment 2
[0043] (1) Dissolve 0.3kg of cellulose in a solution of 6kg of sodium hydroxide and 35kg of water to make a cellulose solution, then heat to 58°C and add 7kg of β-cyclodextrin, stir until completely dissolved, then add 3.5kg of orthosilicon Acetate ethyl ester, then slowly drop into 0.1kg cyclohydrochloropropane and continue to mix and stir to obtain cellulose-modified β-cyclodextrin hydrogel;
[0044] (2) Phosphoric acid was added dropwise to the cellulose-modified β-cyclodextrin hydrogel to adjust the pH value to 1.5, so that tetraethyl orthosilicate was hydrolyzed, and in the interior of the cellulose-modified β-cyclodextrin hydrogel Form silica hydrogel;
[0045] (3) Add the silica hydrogel into water, soak and age for 2 days, after soaking, the hydrogel becomes translucent, and a translucent hydrogel is obtained;
[0046] (4) Freeze-dry the translucent hydrogel at -22°C for 26 hours, and freeze-dry to prepare a silica-complexed β-cyclodextrin aerogel, which is pulverized...
Embodiment 3
[0050] (1) Dissolve 0.4kg of cellulose in a solution of 7kg of sodium hydroxide and 30kg of water to make a cellulose solution, then heat to 62°C and add 8kg of β-cyclodextrin, stir until completely dissolved, then add 4.5kg of orthosilicon Acetate ethyl ester, then slowly drop into 0.12kg cyclohydrochloropropane and continue to mix and stir to obtain cellulose-modified β-cyclodextrin hydrogel;
[0051] (2) Phosphoric acid was added dropwise to the cellulose-modified β-cyclodextrin hydrogel to adjust the pH value to 2.5, so that tetraethyl orthosilicate was hydrolyzed, and in the interior of the cellulose-modified β-cyclodextrin hydrogel Form silica hydrogel;
[0052] (3) Add silica hydrogel to water, soak and age for 3 days, after soaking, the hydrogel becomes translucent, and a translucent hydrogel is obtained;
[0053] (4) Freeze-dry the translucent hydrogel at -18°C for 26 hours, and freeze-dry to prepare a silica-complexed β-cyclodextrin aerogel, which is pulverized for ...
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