Photocatalytic degradation composite particle, and preparation method and application thereof
A composite particle, photocatalytic technology, applied in the field of photocatalysis, can solve problems such as affecting cultivation, aggravation, and difficulty in large-scale use, and achieve the effects of reducing production costs, reducing usage, and strong degradation ability.
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Embodiment 1
[0019] nanoscale anatase TiO 2 Put it in an oven at 110°C for 12 hours and seal it up; put the washed rice straw into a muffle furnace, fully calcinate it at 500°C for 4 hours, collect the ash, put the ash in a grinder and add water to grind it into a homogenate, Filter to remove soluble salt; pass the residue on the filter paper through a 400-mesh sieve under water washing, and collect the sieved particles; suspend the sieved particles in the container, settle naturally for 10 minutes, and then remove the upper suspension; repeat 6 times After the natural precipitation process, pure silica particles are obtained; after peeling the corn stalks, cut them into 1 cm long cylinders, soak them in 10% dilute hydrochloric acid for 48 hours, and then wash them repeatedly with distilled water until the chloride ions are washed away. Then dried at 80°C for 24h, soaked in FeVO 4 In the gel, vacuumize for 30min, take it out after standing for 4h, and dry it at 80°C; put it in a muffle fu...
Embodiment 2
[0021] nanoscale anatase TiO 2 Put it in an oven at 110°C for 12 hours and seal it up; put the washed rice straw into a muffle furnace, fully calcinate it at 500°C for 6 hours, collect the ash, put the ash in a grinder and add water to grind it into a homogenate, Remove the soluble salt by filtration; pass the residue on the filter paper through a 400-mesh sieve under water washing, and collect the sieved particles; suspend the sieved particles in the container, settle naturally for 15 minutes, and then remove the upper suspension; repeat 8 times After the natural precipitation process, pure silica particles are obtained; after peeling the corn stalks, cut them into 1 cm long cylinders, soak them in 10% dilute hydrochloric acid for 48 hours, and then wash them repeatedly with distilled water until the chloride ions are washed away. Then dried at 80°C for 24h, soaked in FeVO 4 In the gel, vacuumize for 30 minutes, take it out after standing for 4 hours, and dry it at 80°C; put...
Embodiment 3
[0023] nanoscale anatase TiO 2 Put it in an oven at 110°C for 12 hours and seal it up; put the washed rice straw into a muffle furnace, fully calcinate it at 500°C for 5 hours, collect the ash, put the ash in a grinder and add water to grind it into a homogenate, Filter to remove soluble salt; pass the residue on the filter paper through a 400-mesh sieve under water washing, and collect the sieved particles; suspend the sieved particles in the container, settle naturally for 10 minutes, and then remove the upper suspension; repeat 7 times After the natural precipitation process, pure silica particles are obtained; after peeling the corn stalks, cut them into 1 cm long cylinders, soak them in 10% dilute hydrochloric acid for 48 hours, and then wash them repeatedly with distilled water until the chloride ions are washed away. Then dried at 80°C for 24h, soaked in FeVO 4 In the gel, vacuumize for 30 minutes, take it out after standing for 4 hours, and dry it at 80°C; put it in a...
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