Gravity adsorption type test rod for rapidly detecting content of chloride ions in sandstone material, preparation method and application thereof
A technology of chloride ion content and sand and gravel materials, which is applied in the direction of analyzing materials through chemical reactions, material analysis and sampling devices through observation of the impact on chemical indicators, etc., can solve the problems of poor portability, time-consuming and laborious, and practical Inconvenient and other problems, to achieve the effect of low cost, good adsorption effect, fast and accurate detection
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Embodiment 1
[0024] A new gravity adsorption test rod for rapid detection of chloride ion content in sand and gravel materials, such as figure 1 and figure 2 As shown, it includes a test rod 2 and a hard plastic case 1 with scales. The test rod 2 is wrapped inside a hard plastic casing 1 with scales, one end of the hard plastic casing 1 is closed for fixing the test rod 2, and the other end is open.
[0025] The test rod 2 is composed of the following materials by weight: cotton fiber, color-changing silica gel, silver chromate, polycarboxylate water reducer and other materials. The shape of the test rod 2 is cylindrical, the length is 50 mm, and the diameter is 10 mm.
[0026] The hard plastic shell 1 is a hollow cylinder with an inner diameter of 10mm, an outer diameter of 12mm and a length of 62mm. The hard plastic shell 1 is made of transparent hard plastic, and its surface is printed with scale lines for reading the discoloration length of the test rod 2 inside it.
[0027] One e...
Embodiment 2
[0029] A method for preparing a gravity adsorption test rod for quickly detecting the content of chloride ions in sand and gravel materials, the details are as follows:
[0030] (1) Prepare 300 mL of silver chromate solution with a mass concentration of 5 g / L, put it into a beaker, and then add water-absorbing silica gel and 0.05 g of polycarboxylate water reducer.
[0031] (2) Weigh 5.9 g of cotton fiber and soak it in the solution prepared in (1) for 1 min.
[0032] (3) Stir the solution described in (2) for 10 min with a stirrer at a speed of 1000 r / min to make a cotton fiber composite base core.
[0033] (4) Put the cotton fiber composite base core prepared in (3) into a mold and vibrate for 3 minutes, then place it in a blast drying oven, and dry it at a temperature of 50°C.
[0034] (5) Weigh 0.5 g of color-changing silica gel, and evenly apply it on the surface of one end of the dried product obtained in (4) to obtain the final product.
[0035] (6) Put the final prod...
Embodiment 3
[0037] A method for detecting chloride ion content in sand and gravel slurry. Use a straw to absorb the filtrate filtered from the sand and gravel material, and then drop the filtrate into the vertically placed test rod through the open end, and the color-changing silica gel at the bottom of the test rod will change color. Finally, read the discoloration length of the test rod and compare it with the discoloration length data of the sample, so as to obtain the chloride ion content in the sand and gravel slurry. details as follows:
[0038] (1) suck the filtrate filtered out from the gravel material with a straw;
[0039] (2) Put the test rod vertically, with the open end facing up, and slowly drop the filtrate in the straw into the open end of the test rod;
[0040] (3) When the filtrate is dripped, observe the discoloration of the discoloration silica gel at the bottom of the test rod;
[0041] (4) When the color-changing silica gel at the bottom of the test rod turns red, ...
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