Water plugging agent, preparation method and application thereof
A technology of water blocking agent and plasticizer, which is applied in chemical instruments and methods, earthwork drilling, wellbore/well parts, etc., and can solve the problems of complex synthesis process, high cost, and high residue content
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Embodiment 1
[0034] The present invention provides a synthesis scheme of a selective water shutoff agent for oil and gas wells used in 40°C reservoirs, including the following steps:
[0035]Step 1: Since the melting temperature of the oil-soluble resin is between 130-140°C, but burning may occur when the melting temperature is higher than 200°C, in order to shorten the melting time, save energy and ensure production safety, the 65 % of the oil-soluble resin is melted when heated to 180°C-200°C;
[0036] Step 2: After the oil-soluble resin is completely melted into a liquid state, add 25% plasticizer, stir evenly, and add 0.7% cross-linking agent under stirring conditions;
[0037] Step 3: In order to ensure that the cross-linking agent is fully mixed, fully reacted and saves energy consumption, the stirring reaction time is controlled between 30-50 minutes, which can be adjusted according to the actual production situation, and then add 4% softening point regulator and stir Uniform, in o...
Embodiment 2
[0045] A synthetic scheme of a selective water shutoff agent for oil and gas wells used in 150°C reservoirs, comprising the following steps:
[0046] Step 1: Since the melting temperature of the oil-soluble resin is between 130-140°C, but when the melting temperature is higher than 200°C, it may burn, so in order to shorten the melting time, save energy and ensure production safety, 90% The oil-soluble resin is melted when heated to 180°C-200°C;
[0047] Step 2: After the oil-soluble resin is completely melted, add 3% plasticizer, stir evenly, and add 1% crosslinking agent under stirring condition;
[0048] Step 3: In order to ensure that the cross-linking agent is fully mixed, fully reacted and saves energy consumption, the stirring reaction time is controlled between 40-70 minutes, which can be adjusted according to the actual production situation, and then 2% softening point regulator is added and stirred Uniform, in order to ensure that the system state has good fluidity ...
Embodiment 3
[0054] A method for preparing a selective water shutoff agent for oil and gas wells used in 100°C reservoirs, comprising the following steps:
[0055] Step 1: Since the melting temperature of the oil-soluble resin is between 130-140°C, but when the melting temperature is higher than 200°C, combustion may occur, so in order to shorten the melting time, save energy and ensure production safety, the 83 % of the oil-soluble resin is melted when heated to 180°C-200°C;
[0056] Step 2: After the oil-soluble resin is completely melted, add 8% plasticizer, stir evenly, and add 0.7% crosslinking agent under stirring condition;
[0057] Step 3: In order to ensure that the cross-linking agent is fully mixed, fully reacted and energy-saving, the stirring reaction time is controlled between 40-70 minutes, which can be adjusted according to the actual production situation, and then add 4% softening point regulator, Stir evenly, in order to ensure that the system has good fluidity at this t...
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