Biomass fermentation broth lubricant for drilling fluid, and preparation method thereof
A technology for biomass fermentation and drilling fluid, which can be used in drilling compositions, chemical instruments and methods, etc., and can solve the problems of environmental pollution and high cost.
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Embodiment 1
[0035] Take the microbial fermentation liquid and remove impurities through 3000r / min high-speed centrifugation for 15min, and take the centrifuged upper layer homogeneous liquid for subsequent use; in parts by weight, get 8 parts of the prepared upper layer homogeneous liquid and place them in a reaction vessel, and then pour them into the reaction vessel Add 3 parts of methanol and 2 parts of p-toluenesulfonic acid in sequence, and carry out esterification reaction for 5 hours under the conditions of 70°C and 400r / min to obtain a crude biomass fermentation solution; the crude biomass fermentation solution is subjected to natural sedimentation , divided into two layers, the lower layer is the water phase, and the upper oil phase is the biomass fermentation broth.
[0036] Add 75 parts by weight of biomass fermentation liquid; 8 parts by weight of potassium oleate; 3 parts by weight of alkylphenol polyoxyethylene ether into the reactor, and react for 4 hours at 70°C and 500r / mi...
Embodiment 2
[0038] 80 parts by weight of the biomass fermentation broth prepared in Example 1; 9 parts by weight of potassium oleate; 4 parts by weight of alkylphenol polyoxyethylene ether were added to the reactor, at 70 ° C, 450r / min conditions After reacting for 3 hours, a biomass fermentation fluid lubricant for drilling fluid was prepared.
Embodiment 3
[0040] 85 parts by weight of the biomass fermentation liquid prepared in Example 1; 10 parts by weight of potassium oleate; After reacting for 3 hours, a biomass fermentation fluid lubricant for drilling fluid was prepared.
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