A kind of preparation method of silver-loaded activated carbon antibacterial fiber membrane
A silver-loaded activated carbon and antibacterial fiber technology, which is applied in the field of fiber membranes, can solve the problems of large specific surface area, poor membrane mechanical properties, and low membrane pressure, and achieve the effects of improving antibacterial performance, good fire resistance, and improving antibacterial properties
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Embodiment 1
[0019] Such as figure 1 A kind of preparation method of shown antibacterial silver-loaded activated carbon, comprises the following steps:
[0020] Step 1) Preparation of antibacterial silver-loaded activated carbon: Weigh a certain amount of activated carbon and soak it in AgNO with a concentration of 0.08mol / L 3 In the solution; choose phosphate as the anti-flocculation agent, take a certain amount of anti-flocculation agent according to the ratio of anti-flocculation agent: silver ion mass ratio of 0.2:1, dissolve in AgNO under ultrasonic conditions 3 solution; then the glucose solution was slowly added dropwise to the stirred AgNO 3 In the solution, heat in a water bath at 60°C and stir magnetically for 24 hours; filter the product, wash it with water several times to remove excess glucose until Ag+ is completely removed, then dry it in vacuum at 70°C for 8 hours; then dry the product in a blast oven at 70°C for 2 hours , and then burn at high temperature in a nitrogen a...
Embodiment 2
[0024] Such as figure 1 A kind of preparation method of shown antibacterial silver-loaded activated carbon, comprises the following steps:
[0025] Step 1) Preparation of antibacterial silver-loaded activated carbon: Weigh a certain amount of activated carbon and soak it in AgNO with a concentration of 0.08mol / L 3 In the solution; choose phosphate as the anti-flocculation agent, take a certain amount of anti-flocculation agent according to the ratio of anti-flocculation agent: silver ion mass ratio of 0.5:1, dissolve in AgNO under ultrasonic conditions 3 solution; then the glucose solution was slowly added dropwise to the stirred AgNO 3 In the solution, heat in a water bath at 60°C and stir magnetically for 24 hours; filter the product, wash it with water several times to remove excess glucose until Ag+ is completely removed, then dry it in vacuum at 70°C for 8 hours; then dry the product in a blast oven at 70°C for 2 hours , and then burn at high temperature in a nitrogen a...
Embodiment 3
[0029] Such as figure 1 A kind of preparation method of shown antibacterial silver-loaded activated carbon, comprises the following steps:
[0030] Step 1) Preparation of antibacterial silver-loaded activated carbon: Weigh a certain amount of activated carbon and soak it in AgNO with a concentration of 0.08mol / L 3 In the solution; choose phosphate as the anti-flocculation agent, take a certain amount of anti-flocculation agent according to the ratio of anti-flocculation agent: silver ion mass ratio of 1:1, and dissolve it in AgNO under ultrasonic conditions. 3 solution; then the glucose solution was slowly added dropwise to the stirred AgNO 3 In the solution, heat in a water bath at 60°C and stir magnetically for 24 hours; filter the product, wash it with water several times to remove excess glucose until Ag+ is completely removed, then dry it in vacuum at 70°C for 8 hours; then dry the product in a blast oven at 70°C for 2 hours , and then burn at high temperature in a nitr...
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