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A kind of high-efficiency antibacterial fiber and its manufacturing method

A technology of antibacterial fiber and manufacturing method, which is applied in the field of textile fibers, can solve the problems of complex preparation conditions and low silver loading of micron-sized silver-loaded molecular sieves, and achieve green industrial production, high-efficiency antibacterial effect, and small size.

Active Publication Date: 2021-06-01
MINJIANG UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The present invention provides a high-efficiency antibacterial fiber and its manufacturing method in view of the shortcomings of the existing blending processing technology, such as the need to use organic solvents and the preparation conditions of micron-sized silver-loaded molecular sieves, the preparation conditions are complex, and the silver-loaded amount is not high.

Method used

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  • A kind of high-efficiency antibacterial fiber and its manufacturing method

Examples

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Comparison scheme
Effect test

Embodiment 1

[0031] Example 1 Manufacture of a high-efficiency antibacterial polyester fiber

[0032] (1) Preparation of nanoscale silver-loaded molecular sieves: at room temperature, in beaker A, dissolve 7g of sodium hydroxide in 25g of deionized water, then add 0.5g of aluminum powder, and stir until the aluminum powder is completely dissolved; in beaker B, Dissolve 4g of sodium hydroxide in 25g of deionized water, then add 35g of silica sol, and stir until the solution becomes clear; under stirring conditions, add the solution in beaker A to beaker B dropwise, and then add 0.2g of AgNO 3 , after continuing to stir for 24 hours, transfer to an oven at 80°C for crystallization for 1 day, centrifuge at 20,000r / min, wash with water to pH 8~9, dry to obtain sample powder, and set aside; the prepared silver-loaded molecular sieve has a specific surface area of ​​780m 2 / g; the size range of particle size is 40~50nm; the pore size mainly includes micropore and mesopore. ;

[0033] (2) Prepa...

Embodiment 2

[0037] Example 2 Manufacture of a high-efficiency antibacterial nylon fiber

[0038](1) Preparation of nanoscale silver-loaded molecular sieves: at room temperature, in beaker A, dissolve 7g of sodium hydroxide in 25g of deionized water, then add 0.5g of aluminum powder, and stir until the aluminum powder is completely dissolved; in beaker B, Dissolve 4g of sodium hydroxide in 25g of deionized water, then add 50g of silica sol, and stir until the solution becomes clear; under stirring conditions, add the solution in beaker A to beaker B dropwise, and then add 0.2g of AgNO 3 , continue stirring for 24 hours, transfer to an oven at 80°C for crystallization for 1 day, centrifuge at 20,000r / min, wash with water to pH 8~9, dry to obtain sample powder, and set aside; the prepared silver-loaded molecular sieve has a specific surface area of ​​760m 2 / g; the size range of particle size is 40~50nm; the pore size mainly includes micropore and mesopore. ;

[0039] (2) Preparation of an...

Embodiment 3

[0043] Example 3 Manufacture of a high-efficiency antibacterial polypropylene fiber

[0044] (1) Preparation of nanoscale silver-loaded molecular sieves: at room temperature, in beaker A, dissolve 7g of sodium hydroxide in 25g of deionized water, then add 0.5g of aluminum powder, and stir until the aluminum powder is completely dissolved; in beaker B, Dissolve 4g of sodium hydroxide in 25g of deionized water, then add 65g of silica sol, and stir until the solution becomes clear; under stirring conditions, add the solution in beaker A to beaker B dropwise, and then add 0.2g of AgNO 3 , continue to stir for 24 hours, transfer to an oven at 80°C for crystallization for 1 day, centrifuge at 20,000r / min, wash with water to pH 8~9, dry to obtain sample powder, and set aside; the prepared silver-loaded molecular sieve has a specific surface area of ​​720m 2 / g; the size range of particle size is 40~50nm; the pore size mainly includes micropore and mesopore. ;

[0045] (2) Preparati...

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Abstract

The invention discloses a high-efficiency antibacterial fiber and a manufacturing method thereof, which mainly includes three steps of preparing antibacterial masterbatch, antibacterial fiber and antibacterial FDY silk. The present invention utilizes nanoscale silver-loaded molecular sieves with small crystal size, large specific surface area, and high silver loading to prepare high-efficiency antibacterial fibers. The content of antibacterial agents (nanoscale silver-loaded molecular sieves) in the fibers is ≤1‰, and the antibacterial rate is over 99%. After repeated washing, the antibacterial effect did not decrease significantly, and the preparation process of the antibacterial fiber does not require the use of organic solvents. The nano-scale silver-loaded molecular sieves used are prepared by a one-pot method without adding any organic templates. The process is simple, low-cost, and green. ,Environmental friendly.

Description

technical field [0001] The invention belongs to the technical field of textile fibers, and in particular relates to a high-efficiency antibacterial fiber and a manufacturing method thereof. Background technique [0002] With the development of science and technology and the improvement of the quality of life, people's health awareness of environmental sanitation is increasing, and the requirements for functional fibers are getting higher and higher. Fibrous woven products (such as towels, underwear, rags, etc.) are indispensable items in daily life. Because they are often in a wet state during use, they are favorable places for the reproduction and reproduction of many pathogenic bacteria, so they also become a source of bacteria transmission. one of the carriers. [0003] Silver ions have the characteristics of high-efficiency antibacterial, high safety, and good compatibility, and are often used as the main component of antibacterial fibers. The existing method is often ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F1/10D01F6/92D01F6/90D01F6/46D01F8/14D01F8/12D01D5/08D01D5/12D01D10/02
CPCD01D5/08D01D5/12D01D10/02D01F1/103D01F6/46D01F6/90D01F6/92D01F8/12D01F8/14
Inventor 郭永梅郭海玲余礼卫赵蕾
Owner MINJIANG UNIV
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