Additive for nonaqueous electrolyte solutions, nonaqueous electrolyte solution, and lithium ion secondary battery
A non-aqueous electrolyte and additive technology, applied in the direction of non-aqueous electrolyte batteries, secondary batteries, non-aqueous electrolytes, etc., can solve the problems of cost increase, low ion conductivity, battery performance deterioration, etc., and improve safety Effect
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Embodiment 1
[0142] Make LiPF in a carbonate mixed solvent (ethylene carbonate: ethyl methyl carbonate = 1:3 (volume ratio)) 6To the solution obtained by dissolving to 1 mol / L, vinylene carbonate was added to make it 2% by mass and 1-propene-1,3-sultone to be 0.5% by mass, and N-(tert- Butoxycarbonyl)-1,2-phenylenediamine 0.72% by mass to prepare a non-aqueous electrolytic solution.
[0143] The cathode active material (LiCoO 2 , セルシード (registered trademark) C20F, Nippon Chemical Industry Co., Ltd.) 100 parts by mass, conductive agent (acetylene black, DENKA BLACK powder, DENKA Co., Ltd.) 3 parts by mass, binder (polyvinylidene fluoride : PVdF, #7208 (8% NMP solution), 37.5 parts by mass of Kureha) and 13.2 parts by mass of NMP (manufactured by Mitsubishi Chemical Corporation) were mixed to prepare a paste-like positive electrode compound slurry. Next, using a coating device, the positive electrode compound slurry was evenly coated on both sides of a positive electrode current collector ...
Embodiment 2
[0157] Make LiPF in a carbonate mixed solvent (ethylene carbonate: ethyl methyl carbonate = 1:3 (volume ratio)) 6 To the solution obtained by dissolving to 1 mol / L, vinylene carbonate was added to make it 2% by mass and 1-propene-1,3-sultone to be 0.5% by mass, and N-(tert- Butoxycarbonyl)-1,3-phenylenediamine 0.72% by mass to prepare a non-aqueous electrolytic solution.
[0158] The cathode active material (LiCoO 2 , セルシード (registered trademark) C8hV, manufactured by Nippon Chemical Industry Co., Ltd.) 100 parts by mass, conductive agent (acetylene black, DENKA BLACK powder, manufactured by DENKA Co., Ltd.) 3 parts by mass, binder (polyvinylidene fluoride : PVdF, #7208 (8% NMP solution), 37.5 parts by mass of Kureha) and 13.2 parts by mass of NMP (manufactured by Mitsubishi Chemical Corporation) were mixed to prepare a paste-like positive electrode compound slurry. Next, using a coating device, the positive electrode compound slurry was evenly coated on both sides of a posi...
Embodiment 3
[0163] Except having used N-(tert-butoxycarbonyl)-1,4-phenylenediamine as an additive, the sample E for short-circuit tests was produced by the method similar to Example 2.
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