Asphalt reinforced foam plugging agent suitable for selective water plugging of oil-water well and preparation method and application thereof
A selective, oil-water well technology, applied in chemical instruments and methods, earthwork drilling, wellbore/well components, etc., can solve problems such as complex process, high implementation cost, and inability to fully exert the performance of plugging agents, reaching the applicable level Extensive, enhanced strength and elasticity, good filling effect
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Embodiment 1
[0034]Example 1 A bitumen-enhanced foam water plugging agent suitable for selective water plugging and profile control of oil and water wells
[0035]Composition: (mass percentage)
[0036]Petroleum pitch (softening point 40℃): 65%
[0037]Foaming agent: 1.5%
[0038]Toluene: 33.5%
[0039]Nitrogen content: 80%
[0040]Prepared by the following method:
[0041]1) Heat the petroleum pitch to soften it and heat it to a molten state;
[0042]2) Prepare a surfactant solution, add a foaming agent to toluene for agitation reaction to obtain a surfactant solution;
[0043]3) Mix and stir molten petroleum pitch and surfactant solution;
[0044]4) Step 3) The obtained molten petroleum asphalt and surfactant solution mixture is filled with nitrogen and stirred, and a large number of tiny, uniform and stable bubbles are generated during the stirring process to obtain asphalt reinforced foam.
Embodiment 2
[0045]Example 2 A bitumen-enhanced foam water plugging agent suitable for selective water plugging and profile control of oil and water wells
[0046]Composition: (mass percentage)
[0047]Petroleum asphalt (softening point 40℃): 40%
[0048]Foaming agent: 2.5%
[0049]Carbon tetrachloride: 57.5%
[0050]Carbon dioxide content: 90%
[0051]Prepared by the following method:
[0052]1) Heat the petroleum pitch to soften it and heat it to a molten state;
[0053]2) Prepare a surfactant solution, add a foaming agent to carbon tetrachloride to perform a stirring reaction to obtain a surfactant solution;
[0054]3) Mix and stir molten petroleum pitch and surfactant solution;
[0055]4) Step 3) The obtained molten petroleum asphalt and surfactant solution mixture is filled with carbon dioxide and stirred. A large number of tiny, uniform and stable bubbles are generated during the stirring process to obtain a reinforced asphalt foam.
Embodiment 3
[0056]Example 3 A bitumen-enhanced foam water plugging agent suitable for selective water plugging and profile control of oil and water wells
[0057]Composition: (mass percentage)
[0058]Petroleum asphalt (softening point 40℃): 55%
[0059]Foaming agent: 1.0%
[0060]Toluene: 44%
[0061]Carbon dioxide and nitrogen mixed gas content: 70%
[0062]Prepared by the following method:
[0063]1) Heat the petroleum pitch to soften it and heat it to a molten state;
[0064]2) Prepare a surfactant solution, add a foaming agent to toluene to perform a stirring reaction to obtain a surfactant solution;
[0065]3) Mix and stir molten petroleum pitch and surfactant solution;
[0066]4) Step 3) The obtained molten petroleum pitch and surfactant solution mixture is fed with a carbon dioxide gas and nitrogen mixed gas and stirred. A large number of tiny, uniform and stable bubbles are generated during the stirring process to obtain a reinforced asphalt foam.
[0067]The asphalt-reinforced foam prepared in the above three embodim...
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