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359results about How to "Temperature resistant" patented technology

Cellulose acetate nanofiltration membrane and preparing method thereof

The invention discloses a cellulose acetate nanofiltration membrane and a preparing method thereof. The preparing method of the cellulose acetate nanofiltration membrane includes the steps that cellulose acetate serves as a raw material, an organic metal framework compound and a small molecule pore-forming agent serve as a mixed additive, the raw material and the mixed additive are dissolved through a solvent to prepare a cellulose acetate membrane casting solution, a dry and clean glass plate with a supporting layer is coated with the prepared membrane casting solution to form a plate nascent-state membrane or the prepared membrane casting solution and a medium with an inner fiber cavity are extruded through a spinneret plate to obtain a hollow fiber nascent-state membrane, the hollow fiber nascent-state membrane is solidified and subjected to heat treatment, and the cellulose acetate nanofiltration membrane is prepared. As the cellulose acetate nanofiltration membrane is prepared through the organic metal framework compound, the porosity factor of the cellulose acetate nanofiltration membrane is increased, and the water flux is improved; the amine-modified organic metal framework compound is introduced into the formula of the membrane casting solution of the cellulose acetate, the nanofiltration membrane can show charged positive electricity after cross-linking, separation of amino acid with positive charges and protein with positive charges can be promoted, and the reject rate of the nanofiltration membrane is increased.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Borosiloxane and preparation method thereof

The invention relates to borosiloxane and a preparation method thereof. According to the method, a hydrolysis solvent and a boron compound are mixed proportionally and added to a reactor, the temperature keeps from 10 DEG C to 35 DEG C, and a mixed monomer is slowly dropwise added under the stirring condition for a hydrolysis reaction; the dropwise-adding time is controlled in 3-6 hours, the reactor is slowly heated to the temperature ranging from 55 DEG C to 65 DEG C after the dropwise-adding is finished, a stirring reaction is performed for 1 hour, and still standing is performed; acid water on the lower layer is separated and neutralized to be neutral, a saturated NaCl solution is used for washing, and an oil phase material is obtained; reduced pressure distillation is performed to remove the solvent, a catalyst I is added, the mixture is heated to 110-130 DEG C, and the rearrangement reaction is performed for 3-5 hours; the mixture is heated to 150-160 DEG C, the splitting cyclization reaction is performed for 2-5 hours, the reaction is finished, the mixture is cooled, and a polyborosiloxane prepolymer is obtained; an end-capping reagent and a catalyst II are added to a system and heated to 110-130 DEG C, and react for 2-4 hours; and pressure is reduced to remove a low-boiling-point substance, and a polyborosiloxane resin is obtained. The borosiloxane and the preparation method have the advantages of good temperature resistance, ageing resistance, impact resistance, toughness and low-temperature flexibility, high adhesion and the like.
Owner:上海爱世博有机硅材料有限公司

Resistance reducing agent for fracturing quick water of shale gas and preparation method thereof

The invention relates to a resistance reducing agent for fracturing quick water of a shale gas and a preparation method thereof. The resistance reducing agent for fracturing quick water of the shale gas is formed by reverse emulsion polymerization by means of combination of a water phase and an oil phase, wherein the weight part ratios of monomers to water in the water phase are sequentially as follows: the ratio of acrylamide: 2-acrylamide-2-methyl propanesulfonic acid: water is (0.7-1.3):(0.7-1.5):1; the weight ratio of monomers to oil in the oil phase is sequentially as follows: the ratio of tween 80:OP-10: white oil is (0.1-0.35):(0.1-0.35):1; and the weight ratio of the water phase to the oil phase is 1:(0.35-0.85). The preparation method comprises the following steps: (1) selecting acrylamide and 2-acrylamide-2-methyl propanesulfonic acid, and dissolving acrylamide and 2-acrylamide-2-methyl propanesulfonic acid in proportion in deionized water to prepare the water phase; (2) selecting tween 80 and white oil and mixing the tween 80 and white oil in a certain proportion to form the oil phase; (3) proportioning the water phase and the oil phase in a certain proportion, and fully mixing to form a stable water-in-oil inverse emulsion base fluid; and (4) catalyzing and initiating by an initiator to synthesize the resistance reducing agent.
Owner:郑州三山石油技术有限公司

Underground gel-forming blocking agent suitable for medium-high temperature high-salt low-permeability reservoirs and preparation method therefor

ActiveCN104974724AStrong ability to delay polycondensation and solidificationEffective blockingDrilling compositionChromatographic separationConcentration ratio
The invention provides an underground gel-forming blocking agent suitable for medium-high temperature high-salt low-permeability reservoirs and a preparation method therefor. By taking the total weight of the blocking agent as reference, the blocking agent comprises the following raw materials: 1% to 4% of water-soluble phenol-formaldehyde resin, 0.5% to 2% of stabilizer, 0 to 10% of flexibilizer and the balance of water. The preparation method of the blocking agent comprises the following steps: selecting the raw materials in proportion, and uniformly mixing so as to obtain the underground gel-forming blocking agent suitable for the medium-high temperature high-salt low-permeability reservoirs. The blocking agent provided by the invention is a homogeneous-phase, transparent and low-viscosity water solution before gel forming; the blocking agent can be selectively injected in a deep stratum water flow preferential migration passage, the shearing, adsorption and chromatographic separation of a stratum for the blocking agent can be ignored, and deep placement does not influence the concentration ratio of the blocking agent; and the polycondensation is delayed at the high temperature in the deep stratum, so that the formed gel has the advantages of high blocking rate, high blocking strength, water flow impact resistance, high temperature resistance and high hydrolysis resistance.
Owner:PETROCHINA CO LTD

Self-lubricating antiseiznig materials and preparing method thereof

InactiveCN1583904AImprove coating application performanceOvercoming the disadvantages of electrostatic sprayingCoatingsFritAtmospheric temperature
This invention adopts the ceramic material and Fluorine resin with moist slippery characteristic to mix altogether, it is wear-resisting to make one, it is warm to be able to bear, corrosion-resistant, do not glue the wear-resisting sizing of pottery of the function. It is become membrane material, ceramic packing, a piece of coating of one pair of groups made up of the solvent and solidification pharmaceutical, succeed the membrane material and include the cellulosic nitric acid ester, gather the acrylic acid. the mixture of three kinds of resin of the polytetrafluoroethylene (PTFE), low-temperature glass dust, the ceramic pcking makes up. Will become membrane material and solvent first while preparing, the solidification pharmaceutical will be mixed evenly, and then put into the ceramic packing, then adopts the disperse the equipment, after mixing evenly, processes in grinding the equipment, sieve, pack. It becomes membrane under normal atmospheric temperature, improve coating coating construction performance, adopt and brush and roll scribbling and spraying, overcome coating must adopt static shortcoming of spraying at present, become low temperature products after the membrane, the high temperature frits again, any little member does not remain materials, has guaranteed this application in the tableware and wear-resisting trade of coating.
Owner:华东船舶工业学院
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