Blackening technology for copper product

A technology for copper products and processes, applied in the field of blackening of copper products, can solve the problems of low physical test requirements, color fading, and high physical test requirements, and achieve good anti-reflection effect.

Pending Publication Date: 2020-12-22
NINGBO POWERMETAL IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, for the blackening treatment of copper products, copper lens or gasket surface, the traditional blackening method used in metal parts is usually adopted. The original blackening line is mainly suitable for the blackening treatment of the surface of auto parts. Salt The fog test and various physical tests have low requirements; the salt spray test and various physical tests of optical lens products have high requirements, and the original blackening process is used for blackening, and the salt spray test and physical dependence test after blackening cannot meet the requirements. According to the customer's technical requirements, copper leakage will occur after more than 90 hours of salt spray test, and discoloration will occur in continuous tests of high temperature, high humidity, thermal shock, and low temperature cold shock

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The invention provides a process for blackening copper products, which is characterized in that it comprises the following steps:

[0029] S1: Degrease and decontaminate at medium temperature. Put the cleaning basket containing the product into the ultrasonic cleaning machine to ensure that the product is completely submerged in the liquid, add a degreasing solution with a ratio of 1:3, heat the temperature to 70°C±10°C, and place the cleaning basket Pull up and down for 2-4 times and start cleaning for 3-5 minutes; the PH value of the degreasing liquid in this step is 11-14; in this step, in order to further improve the degreasing effect, two cleaning machines can be set up side by side for two consecutive times Degreasing cleaning, and the cleaning environment in the two cleaning machines is consistent;

[0030] In addition, during the cleaning process of the ultrasonic cleaning machine, when cleaning copper products such as lenses, a nylon template will be placed in ...

Embodiment 2

[0050] This embodiment has been improved on the basis of Embodiment 1, that is, a hot water rinsing process can be added between steps S10 and S11, and a rinsing tank that can heat the rinsing water can be added. Specifically, the water temperature is maintained at 70 ℃-90 ℃; rinse with hot water to preheat the product in advance and shorten the baking time.

Embodiment 3

[0052] On the basis of Embodiment 1, this embodiment improves the first blackening process and the second blackening process. Specifically, each blackening process includes at least two blackening liquid immersions, and between adjacent two Perform an overflow rinse between the first blackening solution immersion. In this embodiment, the entire blackening process of the product adopts a multi-channel, multiple blackening soaking process in batches to ensure that a uniform and stable blackening film is formed on the surface of the product.

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Abstract

The invention discloses a blackening technology for a copper product. The technology includes the following steps that 1, degreasing and decontaminating are performed, and specifically, stains on thesurface of the product are removed; 2, overflowing and rinsing are performed, and specifically, the stains on the surface of the product are washed; 3, pickling and activating are performed, and specifically, oxides on the surface of the product are removed; 4, overflowing and rinsing are performed, and specifically, the stains are washed; 5, blackening for the first time is performed, and specifically, a light-color blackening layer is formed; 6, overflow and rinsing are performed; 7, blackening for the second time is performed, and specifically, a stable blackening layer is formed; 8, overflow and rinsing are performed; 9, sealing is performed, and specifically, an anti-oxidation film is formed outside the blackening layer of the finished product; 10, overflow and rinsing are performed;11, drying is performed; 12, vibration and grinding are performed to remove dust, and specifically, accumulated dust and impurities on the surface of the product are removed. According to the blackening technology of the copper product, the requirements that the blackening layer of the product does not leak copper in a long-time salt spray test and does not fade for a long time in high-temperature, high-humidity, thermal-shock and low-temperature cold-shock continuous tests can be met, and the product has the good light reflection resistance and refraction resistance.

Description

technical field [0001] The invention relates to the technical field of metal blackening treatment, in particular to a copper product blackening process. Background technique [0002] Blackening (bluening) technology is widely used in the protection and decoration treatment of the surface of tools, measuring tools, fasteners, instruments, mechanical parts, photographic equipment and military products. The traditional blackening process uses a high-temperature alkaline oxidation system containing sodium nitrite, which needs to be treated at about 140°C for 30-90 minutes, or even longer. It also has the disadvantages of high energy consumption, long production cycle, especially the carcinogenic effect of sodium nitrite, poor working conditions, and environmental pollution. Due to these problems, people have devoted themselves to the research and development of the normal temperature blackening process in recent years, and corresponding normal temperature blackening agent produ...

Claims

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Application Information

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IPC IPC(8): C23C22/63C23C22/08C23C22/78C23C22/82
CPCC23C22/63C23C22/08C23C22/78C23C22/82
Inventor 彭功乐邹冰山刘健壮
Owner NINGBO POWERMETAL IND
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