Preparation method of gradient ceramic material
A ceramic material and gradient color technology, which is applied in the field of preparation of gradient color ceramic materials, can solve the problems of easy color fading, unenvironmental protection, poor appearance of ceramic materials, etc.
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preparation example Construction
[0030] refer to figure 1 , a preparation method of gradient color ceramic material comprising:
[0031] Step S1: mixing the azeotropic mixture solvent, dispersant and ceramic powder to obtain a first mixture.
[0032] Specifically, the azeotropic mixture solvent includes at least two of water, ethanol, methyl ethyl ketone, trichloroethylene, toluene, xylene, and ethyl acetate, and the dispersant includes ethoxylates, triethanolamine, fatty amine salts, and fish oil. at least one.
[0033] Step S2: adding a plasticizer and a binder into the first mixture and mixing to obtain a second mixture.
[0034] Specifically, step S2 includes:
[0035] adding a plasticizer and a binder to the first mixture and mixing to obtain the second mixture;
[0036] Or, the plasticizer is covered on the surface of the first mixture, so that the plasticizer forms a plasticizer film on the surface of the first mixture, and the binder is added to the plasticizer film to The binder and the plastici...
Embodiment 1
[0058] Step S1: Add 100 grams of zirconia ceramic powder and 1 gram of ethoxylate into 50 grams of an azeotropic mixture solvent composed of water and ethanol and disperse evenly by ball milling to obtain a first mixture.
[0059] Step S2: Add 1 gram of plasticizer and 2 grams of binder to the first mixture in sequence, specifically, add the plasticizer from the surface of the first mixture so that the plasticizer is on the surface of the first mixture forming a plasticizer film, adding a binder into the plasticizer film, and mixing evenly after the binder is dissolved in the plasticizer to obtain a second mixture.
[0060] Step S3: The second mixture is equally divided into 5 parts, and the colored oxide CoO.Al2O3 is used as a coloring material according to 0.10wt%, 0.15wt%, 0.20wt%, 0.25wt%, 0.30wt% of the zirconia ceramic powder Add to each part of the second mixture in turn, carry out graded ball milling to disperse evenly, ensure that the average particle size D50 of the ...
Embodiment 2
[0065] Step S1: Add 100 grams of zirconia ceramic powder and 1 gram of ethoxylate into 50 grams of an azeotropic mixture solvent composed of water and ethanol and disperse evenly by ball milling to obtain a first mixture.
[0066] Step S2: 1 g of plasticizer and 2 g of binder are simultaneously added to the first mixture and dispersed uniformly by ball milling to obtain a second mixture.
[0067] Step S3: The second mixture is equally divided into 5 parts, and the colored oxide 2CoO.TiO2 is used as a colorant according to 0.10wt%, 0.15wt%, 0.20wt%, 0.25wt%, 0.30wt% of the zirconia ceramic powder The content of each part of the second mixture is added in turn, and the coloring material is configured into a solution and added to 5 parts of the second mixture in a pulse form, the pulse number ratio is 1:2:3:4:5, and the coloring material is obtained by mixing evenly For 5 parts of mixed slurry with different concentrations, the mixed slurry is numbered 2-1, 2-2, 2-3, 2-4, 2-5 in ...
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