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Glass etching solution and method for imitating ceramic furnace transmutation ice flower glass by adopting etching solution

A technology of frosted glass and etching solution, which is applied in glass production, technology for producing decorative surface effects, special decorative structures, etc. It can solve the problems of incomparability and achieve a delicate and smooth surface

Active Publication Date: 2021-02-05
ZHENGZHOU HIHO OPTICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The kiln-transformed ice flower art in ceramics is very popular among collectors. If it is developed to realize the effect of kiln-transformed ice flower on glass artwork or glass ornaments, it will certainly be able to meet the curiosity-seeking needs of the collectors; The way of effect is generally completed by engraving and color painting. This kind of product is reproducible, and it is incomparable with the peerless unique products produced by "Kiln Transformation Wushuang" and "Ten Kiln Nine Transformations" in Jun porcelain.

Method used

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  • Glass etching solution and method for imitating ceramic furnace transmutation ice flower glass by adopting etching solution
  • Glass etching solution and method for imitating ceramic furnace transmutation ice flower glass by adopting etching solution

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The glass etching liquid of the present embodiment is made up of the raw material of following percentage by weight: ammonium fluoride 18.5%, ammonium fluorosilicate 6.8%, magnesium fluorosilicate 3.6%, sulfuric acid 16.2%, acetic acid 4.6%, sodium chloride 6.3%, Lead nitrate 5.2%, sodium pyrophosphate 1.8%, copper sulfate 1.6%, sodium gluconate 0.8%, sodium lauryl sulfate 1.2%, polyacrylamide 0.3%, maltodextrin 0.2%, water 32.9%.

[0029] Adopt above-mentioned glass etchant to prepare the method for frosted glass:

[0030] (1) First accurately weigh the powdery raw materials in the above formula and add them to the reactor, then add the liquid raw materials in the formula to the reactor, adjust the pressure of the reactor to 0.15MPa, the temperature to 50°C, and the stirring speed is 40r / min, and the reaction aging time is 12h, and the etching solution is obtained;

[0031] (2) Take isolation protection for the part of the glass that does not need to be etched, clean ...

Embodiment 2

[0036] The glass etching liquid of the present embodiment is made up of the raw material of following percentage by weight: ammonium fluoride 21.8%, ammonium fluorosilicate 5.8%, magnesium fluorosilicate 3.5%, sulfuric acid 18.5%, acetic acid 3.5%, sodium chloride 7.8%, Lead nitrate 5.6%, sodium pyrophosphate 1.2%, copper sulfate 1.0%, sodium gluconate 1.2%, sodium lauryl sulfate 1.5%, polyacrylamide 0.3%, maltodextrin 0.2%, water 28.1%.

[0037] Adopt above-mentioned glass etchant to prepare the method for frosted glass:

[0038] (1) First accurately weigh the powdery raw materials in the above formula and add them to the reactor, then add the liquid raw materials in the formula to the reactor, adjust the pressure of the reactor to 0.10MPa, the temperature to 55°C, and the stirring speed is 45r / min, and the reaction aging time is 10h, and the etching solution is obtained;

[0039] (2) Take isolation protection for the part of the glass that does not need to be etched, clean ...

Embodiment 3

[0043] The glass etching liquid of the present embodiment is made up of the raw material of following percentage by weight: ammonium fluoride 20.5%, ammonium fluorosilicate 6.0%, magnesium fluorosilicate 4.8%, sulfuric acid 16.5%, acetic acid 3.0%, sodium chloride 8.0%, Lead nitrate 5.0%, sodium pyrophosphate 2.0%, copper sulfate 1.5%, sodium gluconate 1.6%, sodium lauryl sulfate 2.0%, polyacrylamide 0.3%, maltodextrin 0.2%, water 28.6%.

[0044] Adopt above-mentioned glass etchant to prepare the method for frosted glass:

[0045] (1) First accurately weigh the powdery raw materials in the above formula and add them to the reactor, then add the liquid raw materials in the formula to the reactor, adjust the pressure of the reactor to 0.12MPa, the temperature to 55°C, and the stirring speed 50r / min, the reaction aging time is 15h, and the etching solution is obtained;

[0046](2) Take isolation protection for the part of the glass that does not need to be etched, clean the part...

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Abstract

The invention belongs to the technical field of chemical etching, and particularly relates to a glass etching solution and a method for imitating ceramic furnace transmutation ice flower effect glassby adopting the etching solution. The glass etching solution comprises the following raw materials in percentage by weight: 18-25% of ammonium fluoride, 6-10% of ammonium fluosilicate, 2-6% of magnesium fluosilicate, 15-20% of sulfuric acid, 3-8% of acetic acid, 5-10% of sodium chloride, 3-8% of lead nitrate, 1-3% of sodium pyrophosphate, 1-3% of copper sulfate, 0.5-2% of sodium gluconate, 0.5-2.5% of lauryl sodium sulfate, 0.2-0.5% of polyacrylamide, 0.1-0.3% of maltodextrin and the balance of water. According to the etching solution, acid etching treatment is carried out on the surface of the glass so that ice flower-shaped crystals which are different in shape and ever-changing are formed on the surface of the glass.

Description

technical field [0001] The invention belongs to the technical field of chemical etching, and in particular relates to a glass etching solution and a method for preparing glass with an ice effect imitating a ceramic kiln by using the etching solution. Background technique [0002] The kiln-transformed ice flower art in ceramics is very popular among collectors. If it is developed to realize the effect of kiln-transformed ice flower on glass artwork or glass ornaments, it will certainly be able to meet the curiosity-seeking needs of the collectors; The way of effect is generally completed by engraving and painting. This kind of product is reproducible, and it is incomparable with the peerless unique products produced by "Kiln Transformation Wushuang" and "Ten Kiln Nine Transformations" in Jun porcelain. [0003] The present invention adopts acid etching technology to form unpredictable texture patterns and frost effects on the glass surface, so that each product has its own un...

Claims

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Application Information

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IPC IPC(8): C03C15/00B44C1/22B44C5/00
CPCC03C15/00B44C1/227B44C5/00Y02P40/57
Inventor 熊国祥熊钰坤石海亮
Owner ZHENGZHOU HIHO OPTICAL TECH CO LTD
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