Rare earth permanent magnet material and preparation process thereof

A preparation process, rare earth permanent magnet technology, applied in the direction of magnetic materials, inductance/transformer/magnet manufacturing, magnetic objects, etc., can solve the problems of thermal expansion, micro-crack micro-crack expansion, increase the cost of process steps, etc., to achieve good magnetization performance Effect

Pending Publication Date: 2021-02-26
周慧媛
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, since the NdFeB permanent magnet powder used in bonded NdFeB rare earth permanent magnets usually produces microcracks in the magnetic powder particles during the refining and crushing process, resulting in an active surface, it is very easy to oxidize and corrode, so that in the subsequent use process It is easy to cause rapid oxidation and corrosion to cause a sharp drop in magnetic properties, especially in the preparation process of compression molding, it is easier to cause new microcracks and the continuous expansion of original microcracks due to compression
At the same time, thermosetting resins used as binders are usually prone to softening and thermal expansion in high-temperature environments, which in turn causes a series of problems such as the reduction of high-temperature mechanical strength and magnetic properties of bonded NdFeB rare earth permanent magnets.
As mentioned earlier, after forming and curing, it is usually necessary to coat the surface with an anti-corrosion film to solve problems such as anti-corrosion and thermal demagnetization, but this will increase many process steps and a lot of cost

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The bonded rare earth permanent magnet material in the present invention is prepared by the following preparation process:

[0030] 1) According to the mass percentage of Nd 16.0, Ce 7.0, B 0.98, Al 0.6, Cu 0.55, Co 0.1, Zr 5.2, the balance is Fe and unavoidable impurities, prepare the NdFeB magnetic powder raw material, the particle size of the magnetic powder The powder content of less than 40 μm is 50 wt.%, and the powder content of particle size less than 25 μm is 18 wt.%.

[0031] Wherein, not limited to shown in embodiment 1, the Nd and Ce elements in the present invention are the core elements that the main phase in the rare earth permanent magnetic alloy material forms, in order to ensure sufficient formation of R 2 T 14The main phase crystal structure of B, to obtain sufficient magnetic properties, the content of Nd and Ce elements should not be too low, otherwise the coercive force (HcJ) of the material will be too low; but the content of rare earth elements ...

Embodiment 2

[0046] Embodiments 2 and 3 are the same as Embodiment 1 except that the composition of the magnetic powder raw material is different from that of Embodiment. Wherein, in embodiment 2, according to mass percent, be Nd 18.0, Ce 6.5, B 0.96, Al 0.6, Cu 0.50, Co0.1, Zr 5.1, balance is Fe and unavoidable impurity; In embodiment 3, according to mass The percentages are Nd 15.8, Ce 7.8, B 0.99, Al 0.7, Cu 0.55, Co 0.1, Zr 5.0, and the balance is Fe and unavoidable impurities.

Embodiment 4

[0047]In Examples 4 and 5, except for the particle size distribution of the magnetic powder raw material, the others are the same as in Example 1. Wherein, in embodiment 4, the powder content of particle size less than 40 μm in the NdFeB magnetic powder is 30wt.%, and the powder content of particle size less than 25 μm is 17wt.%. In embodiment 5, the particle size of the NdFeB magnetic powder is The powder content of less than 40 μm is 45 wt. % and the powder content of particle size less than 25 μ m is 10 wt. %.

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Abstract

The invention provides an rare earth permanent magnet material and a preparation process thereof. According to the invention, specific permanent magnet alloy powder limited by the ratio of each element is adopted, and an unique binder resin composition is adopted for special granulation, molding and coating treatment to obtain a bonded rare earth permanent magnet material, so that the bonded rareearth permanent magnet material has the advantages of low cost, high temperature resistance, corrosion resistance, excellent magnetizing performance and the like, and the use reliability, stability and wide applicability of the rare earth permanent magnet material are ensured.

Description

technical field [0001] The invention relates to the technical field of magnetic materials, in particular to a bonded rare earth permanent magnet material with low cost, high temperature resistance and excellent magnetization. Background technique [0002] Rare earth permanent magnet materials are permanent magnet alloy materials with intermetallic compounds composed of different rare earth elements and transition group metal elements (Fe, Co, Ni, etc.) as the main phase. Since it was invented in the 1960s, rare earth permanent magnet materials have developed rapidly and have been widely used in many fields. They have become important basic functional materials for contemporary new technologies, especially in the field of permanent magnet motors. effect. Nowadays, rare earth permanent magnet motors have covered various main types such as stepping motors, brushless motors, servo motors and linear motors, and are widely used in computers, printers, household appliances, air-co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F1/057H01F41/02
CPCH01F1/0576H01F1/0578H01F41/0253H01F41/0266
Inventor 周慧媛
Owner 周慧媛
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