Preparation method of blending modified CPET sheet for high-temperature-resistant oven
A technology of blending modification and high temperature resistance, which is applied in the field of preparation of CPET sheets for blending and modified high temperature resistance ovens, can solve the problems of insufficient mechanical strength, resistance to bumps, brittleness, etc., and achieves uniform mechanical strength and no Pollution, improve the effect of thermal storage paste
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[0019] The preparation method of the blended modified CPET sheet for high temperature resistant oven comprises the following steps: taking PET, modified material, phosphoric acid ester dispersant and organic chemical foaming agent as raw materials according to parts by weight; The material is subjected to ultrasonic dispersion treatment; the modified material after ultrasonic dispersion treatment and the remaining raw materials are heated to 180-200°C, mixed for 1-2 hours, and then extruded. The frequency range of the ultrasonic treatment is 20KHz-50KHz, and the power used is 700-1500W.
[0020] In the embodiment of the present invention, PET is used as the main raw material for preparation. PET refers to polyethylene terephthalate, which is a crystalline saturated polyester, and is a milky white or light yellow, highly crystalline polymer with a smooth and shiny surface. It is a common resin in daily life. It has excellent physical and mechanical properties in a wide temperat...
Embodiment 1
[0031] The raw materials are weighed according to the following parts by weight: 100 parts of PET, 5 parts of graphene, 1 part of phosphate ester dispersant, 1 part of organic chemical foaming agent; ultrasonic dispersion treatment is carried out to graphene, and the ultrasonic treatment frequency is a frequency range of 20KHz, And the power used is 700W; the graphene after ultrasonic dispersion treatment and the remaining raw materials are heated to 180°C, mixed for 1 hour, and then extruded. Cut the test sample of 10cm×10cm×10cm, measure its maximum tensile strength and elongation at break by stretching the test sample in the transverse and longitudinal directions; and tear the test sample in the transverse and longitudinal directions to measure the tearing force of the test sample ; Extrude the experimental sample with a pressing force of 100N in the transverse and longitudinal directions, and measure the dimensional change rate of the experimental sample.
Embodiment 2
[0033] The raw materials are weighed according to the following parts by weight: 100 parts of PET, 27 parts of graphene, 3 parts of phosphate ester dispersant, 3 parts of organic chemical foaming agent; ultrasonic dispersion treatment is carried out to graphene, and the frequency range of ultrasonic treatment is 35KHz, And the power used is 1100W; the graphene after the ultrasonic dispersion treatment and the remaining raw materials are heated to 190°C, mixed for 1.5 hours, and then extruded. Cut the test sample of 10cm×10cm×10cm, measure its maximum tensile strength and elongation at break by stretching the test sample in the transverse and longitudinal directions; and tear the test sample in the transverse and longitudinal directions to measure the tearing force of the test sample ; Extrude the experimental sample with a pressing force of 100N in the transverse and longitudinal directions, and measure the dimensional change rate of the experimental sample.
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