A kind of synthetic fatliquoring agent of low atomization leather and its preparation method and application

A fatliquor and low-fogging technology, which is applied in the field of low-fogging leather synthetic fatliquor and its preparation, can solve the problems of high fogging value and VOC

Active Publication Date: 2022-06-03
QI HE LI HOU CHEM CO LTD
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Traditional fatliquors are mostly composed of animal and vegetable oils and their modified products. There are many unsaturated oils, which are easily decomposed by light and heat to cause rancidity and form some volatile components. There are also many volatile components in the raw materials, so the atomization value and higher VOC

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0049] The present invention also provides the preparation method of the low-atomization leather synthetic fatliquor described in the above technical solution, comprising the following steps:

[0050] Mixing N-oleoyl sarcosine, palm oil and neutralizing agent to carry out neutralization reaction to obtain neutralized product;

[0051] Mixing the neutralized product and maleic anhydride, and carrying out an esterification reaction to obtain an esterified product;

[0052] Physically mixing the esterified product with high-boiling point mineral oil, synthetic oil and emulsifier to obtain a mixture;

[0053] The mixture is mixed with water and emulsified to obtain a synthetic fatliquoring agent for low fogging leather.

[0054] In the present invention, N-oleoyl sarcosine, palm oil and neutralizing agent are mixed, and neutralization reaction is carried out to obtain a neutralized product. In the present invention, the method for mixing N-oleoyl sarcosine, palm oil and neutralizi...

Embodiment 1

[0066] In parts by weight, 20 parts of N-oleoyl sarcosine and 50 parts of 24 degree palm oil were added to the reactor, 15 parts of monoethanolamine were added dropwise, and neutralization reaction was carried out for 1 hour to obtain a neutralized product;

[0067] The neutralized product was heated to 100° C., 10 parts of maleic anhydride were added, and an esterification reaction was carried out for 5 hours to obtain an esterified product;

[0068] Add 15 parts of base oil 150BS, 15 parts of polyisobutylene bissuccinimide, 10 parts of 80EO cetyl alcohol polyoxyethylene ether to the esterification product, and mix for 3 hours to obtain a mixture;

[0069] The mixture was cooled to 60°C, 100 parts of distilled water was added, stirred at 80 rpm for 1 hour, then transferred to the emulsification kettle, stirred for 2 hours, the stirring speed of the emulsification kettle was 1800 rpm, and then the temperature was lowered and discharged to obtain a synthetic leather with low ato...

Embodiment 2

[0072] In parts by weight, 40 parts of N-oleoyl sarcosine and 100 parts of 50 degree palm oil were added to the reactor, 30 parts of triethanolamine were added dropwise, and neutralization reaction was carried out for 3 hours to obtain a neutralized product;

[0073] The neutralized product was heated to 120° C., 18 parts of maleic anhydride were added, and an esterification reaction was carried out for 4 hours to obtain an esterified product;

[0074] 20 parts of base oil 250SN, 10 parts of trimethylolpropane oleate, and 10 parts of alkyl glycosides were added to the esterified product, and mixed for 3 hours to obtain a mixture;

[0075] The mixture was cooled to 50°C, 200 parts of distilled water was added, stirred at 160 rpm for 1 hour, then transferred to the emulsification kettle, stirred for 3 hours, and the stirring speed of the emulsification kettle was 4000 rpm, and then the temperature was lowered to discharge to obtain a synthetic leather with low atomization. Fatli...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
boiling pointaaaaaaaaaa
freezing pointaaaaaaaaaa
Login to view more

Abstract

The invention provides a low-atomization leather synthetic fatliquoring agent as well as its preparation method and application, and relates to the technical field of leather chemical industry. The synthetic fatliquoring agent for low atomization leather provided by the present invention, the preparation raw material comprises the following components by weight: 20-40 parts of N-oleoyl sarcosine; 50-100 parts of palm oil; 10-20 parts of maleic anhydride 10-50 parts of high boiling point mineral oil; 10-50 parts of synthetic oil; 5-50 parts of neutralizer; 10-30 parts of emulsifier; 100-200 parts of water. In the raw material components used in the present invention, there are less unsaturated oils and volatile components, and the higher saturation of palm oil is used to further reduce the formation of volatiles through chemical modification, and then matched with high-boiling point mineral oil, thereby reducing fog value and VOC; the low fogging leather synthetic fatliquoring agent provided by the invention is used for automobile upholstery leather, and good low fogging performance can be obtained.

Description

technical field [0001] The invention relates to the technical field of leather chemical industry, in particular to a low-atomization leather synthetic fatliquor and a preparation method and application thereof. Background technique [0002] Fatliquoring is the most critical process in tanning production. By reasonably and properly fatliquoring the raw leather, it can absorb an appropriate amount of fatliquoring material, restore its original softness and elasticity, and prevent the leather from stiffening and cracking. Gives leather a certain performance. Through fatliquoring, the tensile strength, toughness, elongation, and leather yield of the leather are improved, and the water resistance is significantly improved, and the leather is also given a good feel. [0003] With the improvement of people's living standards, cars have entered millions of households, and people's demand for high-end cars is also increasing. The interiors of high-end cars, especially car seat cushi...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): C14C9/02
CPCC14C9/02
Inventor 冯练享王顺平白清泉
Owner QI HE LI HOU CHEM CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap