Dalbergia cochinchinensis small decorative article identification method based on infrared spectrum

A technology of infrared spectroscopy and Dalbergia cochinchinensis, applied in the field of wood identification, can solve the problems of long detection time, widening of absorption band, high cost, etc., and achieve the effect of objective and accurate experimental results, fast analysis speed and small sample size

Pending Publication Date: 2021-04-13
INST OF WOOD INDUDTRY CHINESE ACAD OF FORESTRY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the market, the species of Dalbergia cochinchinensis will be used to counterfeit Dalbergia cochinchinensis, which has brought great troubles and economic losses to lovers and collectors of Dalbergia cochinchinensis handicrafts
[0003] The traditional wood identification method is mainly based on the morphology and arrangement of various types of wood cells and tissues, which are identified through a microscope. This microscopic identification method has many defects: it will damage the sample (1cm needs to be cut when sampling 3 left and right wood samples), the detection is time-consuming and costly, including softening treatment, slicing and dyeing, etc., generally takes 2 weeks, and requires experienced professionals to identify and identify, with a certain degree of subjectivity, and It is currently difficult to identify species
[0004] However, the technology of classifying based on the constituent elements of wood itself needs to rely on laboratory analysis equipment, and most of them need to grind the wood to destroy the integrity of the wood, and the analysis cost is high, the analysis time is long, and experienced analysis is required The personnel judge the results; the existing wood identification technology based on near-infrared spectroscopy needs to process wood samples, and the directly obtained samples are prone to problems such as broadening of the absorption band and affecting its resolution effect when used for detection

Method used

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  • Dalbergia cochinchinensis small decorative article identification method based on infrared spectrum
  • Dalbergia cochinchinensis small decorative article identification method based on infrared spectrum
  • Dalbergia cochinchinensis small decorative article identification method based on infrared spectrum

Examples

Experimental program
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Embodiment 1

[0031] A method for identifying small ornaments of Dalbergia cochinchinensis based on infrared spectroscopy, comprising:

[0032] Step 1: Turn on the infrared lamp, take about 100 mg of spectrally pure potassium bromide and grind it to a particle size of less than 2.5 μm within the irradiation range of the infrared lamp, transfer the powder to the tableting mold, assemble the mold and put it into the tablet as a whole In the machine, a pressure of about 8t is applied, and the pressure is unloaded after about 1min to obtain transparent or translucent potassium bromide flakes. Put the potassium bromide thin slice on the sample holder in the sample chamber of the infrared spectrometer for testing, and the scanning range of the infrared spectrum is set to 4000-400cm -1 , with a spectral resolution of 4 cm -1 , accumulatively scanned 16 times to obtain the infrared spectrum background image of the measured sample.

[0033] Step 2: Scrape about 1-5 mg of wood powder sample from a ...

Embodiment 2

[0037] A method for identifying small ornaments of Dalbergia cochinchinensis based on infrared spectroscopy, comprising:

[0038] Step 1: Turn on the infrared lamp, take about 100 mg of spectrally pure potassium bromide and grind it to a particle size of less than 2.5 μm within the irradiation range of the infrared lamp, transfer the powder to the tableting mold, assemble the mold and put it into the tablet as a whole In the machine, a pressure of about 8t is applied, and the pressure is unloaded after about 1min to obtain transparent or translucent potassium bromide flakes. Put the potassium bromide thin slice on the sample holder in the sample chamber of the infrared spectrometer for testing, and the scanning range of the infrared spectrum is set to 4000-400cm -1 , with a spectral resolution of 4 cm -1 , accumulatively scanned 16 times to obtain the infrared spectrum background image of the measured sample.

[0039] Step 2: Scrape about 1-5 mg of wood powder sample from th...

Embodiment 3

[0043] A method for identifying small ornaments of Dalbergia cochinchinensis based on infrared spectroscopy, comprising:

[0044] Step 1: Turn on the infrared lamp, take about 100 mg of spectrally pure potassium bromide and grind it to a particle size of less than 2.5 μm within the irradiation range of the infrared lamp, transfer the powder to the tableting mold, assemble the mold and put it into the tablet as a whole In the machine, a pressure of about 8t is applied, and the pressure is unloaded after about 1min to obtain transparent or translucent potassium bromide flakes. Put the potassium bromide thin slice on the sample holder in the sample chamber of the infrared spectrometer for testing, and the scanning range of the infrared spectrum is set to 4000-400cm -1 , with a spectral resolution of 4 cm -1 , accumulatively scanned 16 times to obtain the infrared spectrum background image of the measured sample.

[0045] Step 2: Scrape about 1-5 mg of wood powder samples from t...

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Abstract

The invention relates to a dalbergia cochinchinensis small decorative article identification method based on infrared spectrum, and belongs to the technical field of wood identification. The method comprises the steps of 1, grinding and mixing 1-5mg of sample powder of a to-be-detected dalbergia cochinchinensis small decorative article with potassium bromide, pressing into a sample sheet, and preparing a potassium bromide sheet at the same time; 2, firstly testing an infrared spectrum background image, and then testing an infrared spectrogram of the sample; 3, performing coordinate conversion and baseline correction processing on the original spectrum; and 4, comparing the infrared spectrum of the sample with a standard spectrum, and respectively comparing peak positions, shapes, sizes and correlation coefficients of characteristic peaks existing in the infrared spectrum. The method has the advantages of small sample amount, great reduction of the damage to artware, simplicity in operation, objective and accurate experiment result, and realization of the rapid identification of the material of the dalbergia cochinchinensis small decorative article.

Description

technical field [0001] The invention relates to the technical field of wood identification, and specifically provides a method for identifying small ornaments of Dalbergia cochinchinensis based on infrared spectroscopy. Background technique [0002] Dalbergia cochinchinensis, commonly known as Siamese rosewood, is one of the most precious hardwoods in the world. Because of its slow growth, hard texture, beautiful pattern and pleasant smell, it is very popular among people. The small ornaments made of Cochin Dalbergia wood are bright in color and have unique ornamental and collection values. In the market, species similar to Dalbergia cochinchinensis will be used to counterfeit Dalbergia cochinchinensis, which has brought great troubles and economic losses to Dalbergia cochinchinensis handicraft lovers and collectors. [0003] The traditional wood identification method is mainly based on the morphology and arrangement of various types of wood cells and tissues, which are id...

Claims

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Application Information

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IPC IPC(8): G01N21/3563
CPCG01N21/3563G01N2021/3572
Inventor 黄安民付跃进程献宝张方达马芳
Owner INST OF WOOD INDUDTRY CHINESE ACAD OF FORESTRY
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