Method for rapidly determining various pesticide residues in ecological textiles based on liquid chromatography-triple quadrupole-tandem mass spectrometry technology
A triple quadrupole and liquid chromatography technology, applied in measuring devices, instruments, scientific instruments, etc., can solve the problems of low detection sensitivity, long detection cycle, low detection efficiency, etc., achieve high sensitivity, save time, and improve safety sexual effect
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[0056] According to the domestic and foreign requirements for the limit of various pesticide residues in ecological textiles, and in combination with the current situation of pesticide use in the production process of ecological textiles, the technical solution provided in this embodiment is suitable for laboratory testing conditions. At the same time, the qualitative and quantitative methods of rapid screening and detection, and the detection process are as follows:
[0057] 1. Instrument
[0058] Liquid chromatography tandem mass spectrometer (Waters Acquity / AB6500), American Waters Company / American AB Company; cryogenic centrifuge (USA Beckman Coulter Company); Vortex-Genie 2 vortex oscillator (USA Scientific Industries Company); electronic analysis Balance (Sartorius, Germany); electronic analytical balance AE163, Mettler, Switzerland; nitrogen blowing concentrator (Organomation Associates, EVAP 112); Millipore-Elix-QE-QG ultrapure water machine (Millipore, USA).
[0059]...
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