Magnolol microcapsule spray preservative and preparation method thereof
A magnolol and microcapsule technology, which is applied in the field of honokiol microcapsule spray preservative and its preparation, can solve the problems of unstable phenolic substances, short preservation time, complicated operation, etc., and achieves prolonged biological activity and preservation effect. Excellent and safe effect
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Embodiment 1
[0025] (1) Beta-cyclodextrinolysis is soluble in distilled water, mix uniform, prepared β-cyclodecephaly, the mass fraction of β-cyclodextrin in beta-cyclo paste water solution is 10%;
[0026] (2) The thickness is dissolved in the ethanol solution to prepare mixed liquid I; the concentration of phenol in the mixture I is 10%;
[0027] (3) Pour the mixed liquid 1 into the β-cyclodextrous water solution, ultrasonic treatment, and have a thick phenolic microcapsule; the mass ratio of mixed liquid I and β-cyclo passenger water solution is 1: 1; ultrasonic treatment parameters To: The ultrasonic time is 10 min, the ultrasonic power is 120W, the core wall ratio is 1: 1; the buried rate of the thick phenolic microcapsules is 86.162%;
[0028] (4) Disperse the thick phenolic microcapsules in the citrus essential oil, and the spray preservative of the thick and phenolic microcapsules, the mass ratio of the thick phenolic microcapsules and citrus essential oils is 3: 100.
[0029] Characte...
Embodiment 2
[0032] (1) The β-cyclodextrin is dissolved in distilled water, mixed uniform, prepared β-cyclodextrous water solution; the mass fraction of β-cyclodextrin in the β-cyclodextrous solution is 8%;
[0033] (2) Soluble in ethanol solution in ethanol, resulting in mixed liquid I; concentration of phenol in the mixed liquid I is 8%;
[0034] (3) Pour the mixed liquid 1 into the β-cyclodextrous water solution, ultrasonic treatment, and produce a thick phenolic microcapsule; the mass ratio of the mixed liquid I and the β-cyclodextrous water solution is 1: 2; ultrasonic treatment parameters To: Ultrasonic time is 8 minutes, ultrasonic power is 100W, core wall ratio 1: 2; the bubble rate of thick phenolic microcapsules is 70.609%;
[0035] (4) Disperse the thick phenolic microcapsules in citrus essential oils, and the spray preservation agents of the porphenic microcapsules, the mass ratio of the phenoliol microcapsules and citrus essential oils are 2: 100.
[0036] Characterization of the ...
Embodiment 3
[0038] (1) The β-cyclodextrin is dissolved in distilled water, mixed uniform, prepared β-cyclodextrous water solution; the mass fraction of β-cyclodextrin in the β-cyclodextrous solution is 12%;
[0039] (2) The thickness is dissolved in the ethanol solution to prepare mixed liquid 1; the concentration of phenol in the mixture I is 12%;
[0040] (3) Pour the mixed liquid 1 into the beta-cycloMenefic water solution, ultrasonic treatment, and produce thick phenolic microcapsules; the mass ratio of mixed liquid I and β-cyclo paste water solution is 2: 1; ultrasonic treatment parameters To: Ultrasonic time is 12min, ultrasonic power 140W, core wall ratio 2: 1; the buried rate of thick phenolic microcapsules is 50.134%;
[0041] (4) Disperse the thick phenolic microcapsules in the citrus essential oil, and the spray preservative of the phenolic microcapsules, the mass ratio of the thick and phenolic microcapsules and citrus essential oils is 4: 100.
[0042] Characterization of the obt...
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