Graphene PI composite material as well as preparation method and application thereof
A composite material and graphene technology, which is applied in the direction of conductive coating, additive processing, epoxy resin coating, etc., can solve the problem of complex construction process, affecting the appearance smoothness of the subsequent coating process, and poor adhesion between the coating and the middle frame substrate. Stability and other issues, to achieve the effects of excellent signal conduction, excellent substrate adhesion, and excellent electrical and thermal conductivity
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[0031] A kind of preparation method of graphene PI composite material, comprises the steps:
[0032] First add the active monomer to the dispersion tank, and disperse for 10 minutes at a speed of 500 rpm;
[0033] Then add photoinitiator and dispersant, and disperse for 10 minutes at a speed of 500 rpm;
[0034] Then add graphene, disperse for 20 minutes at a speed of 2000 rpm, and then use ultrasonic dispersion to obtain a semi-finished product, and use an electron microscope to detect the fineness of the semi-finished product≤200nm;
[0035] Put the semi-finished product into the disperser, then add high molecular PI composite polymer and leveling agent, disperse for 30 minutes at a speed of 2000 rpm, filter and pack.
[0036] In the step of adding graphene again, dispersing at a speed of 2000 rpm for 20 minutes, then using ultrasonic dispersion to obtain a semi-finished product, and using an electron microscope to detect the fineness of the semi-finished product≤200nm, the...
Embodiment 1
[0039] A graphene PI composite material is composed of the following components by mass percentage: high molecular PI composite polymer 35%; active monomer 50%; photoinitiator 7%; graphene 5%; dispersant 2%; leveling agent 1%.
[0040] A kind of preparation method of graphene PI composite material, comprises the steps: first active monomer is added into dispersing kettle, disperses 10 minutes with the speed of 500 revs / min; Disperse at a speed of 10 minutes; then add graphene, disperse at a speed of 2000 rpm for 20 minutes, then use ultrasonic dispersion for 1.5-2.0 hours to obtain a semi-finished product, and use an electron microscope to detect the fineness of the semi-finished product ≤ 200nm; add the semi-finished product to the disperser , and then add high-molecular PI composite polymer and leveling agent, disperse for 30 minutes at a speed of 2000 rpm, filter and pack.
Embodiment 2
[0042] A graphene PI composite material is composed of the following components by mass percentage: high molecular PI composite polymer 40%; active monomer 45%; photoinitiator 7%; graphene 5%; dispersant 2%; leveling agent 1%.
[0043] A kind of preparation method of graphene PI composite material, comprises the steps: first active monomer is added into dispersing kettle, disperses 10 minutes with the speed of 500 revs / min; Disperse at a speed of 10 minutes; then add graphene, disperse at a speed of 2000 rpm for 20 minutes, then use ultrasonic dispersion for 1.5-2.0 hours to obtain a semi-finished product, and use an electron microscope to detect the fineness of the semi-finished product ≤ 200nm; add the semi-finished product to the disperser , and then add high-molecular PI composite polymer and leveling agent, disperse for 30 minutes at a speed of 2000 rpm, filter and pack.
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