Recyclable pH value responsive reversible emulsifier for oil field drilling fluid
An oil field drilling and responsive technology, applied in drilling compositions, chemical instruments and methods, etc., can solve problems affecting the reversible transformation performance of emulsions, poor temperature resistance and shear resistance, and the limited number of reversible transformations of reversible emulsifiers. And other issues
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Embodiment 1
[0037] Embodiment 1, the recyclable pH value responsive reversible emulsifier for oil field drilling fluid mentioned in the present invention, its preparation method comprises the following steps, and each component is by weight:
[0038] The first step is to coat the surface with SiO 2 layer of Fe 3 o 4 @SiO 2 Synthesis of Magnetic Nanoparticles
[0039] Take 1.5 parts of Fe 3 o 4 Add nanoparticles to 150 parts of absolute ethanol, stir at a constant speed of 200r / min for 10min, and disperse with ultrasonic at room temperature for 30min to obtain a fully dispersed suspension; Nitrogen was passed for 0.5h under stirring conditions, during which the pH was continuously monitored with a pH meter and the pH of the suspension was adjusted to neutral with 2mol / L HCl solution, then 3mL of 7% TEOS solution was slowly added dropwise, and the pH was adjusted to 9 after continuous stirring for 10min , continue to stir for 12 hours and then end the reaction. After the product is wa...
Embodiment 2
[0045] Embodiment 2, the recyclable pH value responsive reversible emulsifier for oil field drilling fluid mentioned in the present invention, its preparation method comprises the following steps, and each component is by weight:
[0046] The first step is to coat the surface with SiO 2 layer of Fe 3 o 4 @SiO 2 Synthesis of Magnetic Nanoparticles
[0047] Take 0.5 parts of Fe 3 o 4 Add nanoparticles to 150 parts of absolute ethanol, stir at a constant speed of 180r / min for 8min, and disperse by ultrasonic at room temperature for 30min to mix evenly to obtain a fully dispersed suspension. Nitrogen was passed for 0.5h under stirring conditions, during which the pH was continuously monitored with a pH meter and the pH of the suspension was adjusted to neutral with 2mol / L HCl solution, then 3mL of 7% TEOS solution was slowly added dropwise, and the pH was adjusted to 9 after continuous stirring for 10min , continue to stir for 12 hours and then end the reaction. After the pr...
Embodiment 3
[0053] Embodiment 3, the recyclable pH value responsive reversible emulsifier for oil field drilling fluid mentioned in the present invention, its preparation method comprises the following steps, and each component is calculated by weight
[0054] The first step is to coat the surface with SiO 2 layer of Fe 3 o 4 @SiO 2 Synthesis of Magnetic Nanoparticles
[0055] Take 1.5 parts of Fe 3 o 4 Add nanoparticles to 150 parts of absolute ethanol, stir at a constant speed of 200r / min for 10min, and disperse with ultrasonic at room temperature for 30min to obtain a fully dispersed suspension. Under the condition of stirring, nitrogen gas was passed for 0.5 h, during which the pH was continuously monitored with a pH meter and the pH of the suspension was adjusted to neutral with 2 mol / L HCl solution, and then 3 mL of 7% TEOS solution was slowly added dropwise. After continuing to stir for 10 minutes, adjust the pH to 9, and continue to stir for 12 hours to end the reaction. Aft...
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