Composition containing pyraclonil and pretilachlor
A technology of bisflufenacil and a composition is applied in the field of herbicide preparation and can solve the problems of reduced rice yield, rice death and the like
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Embodiment 1
[0040] A composition containing dipacenil and pretilachlor, which is prepared by curing the microcapsule liquid coated with the core material;
[0041] The composition is made by the following steps:
[0042] Step S1: adding the core material and the microcapsule liquid into a stirred tank, stirring for 20 seconds at a rotating speed of 5000 r / min, and then stirring for 15 minutes at a rotating speed of 400 r / min to obtain a mixed solution;
[0043] Step S2: Add the mixed solution into the stirred tank, adjust the pH value to 5, add glutaraldehyde solution, stir for 10 minutes, and keep the temperature at 30°C for 30 minutes, filter and remove the filtrate, and dry the filter cake to prepare get the composition.
[0044] The microcapsule fluid wherein is made by following steps:
[0045] Step A1: Add tetrahydrofuran, acetophenone and phenylmagnesium bromide into the reaction kettle, and react for 4 hours under the conditions of rotation speed of 150r / min and temperature of 50°...
Embodiment 2
[0054] A composition containing dipacenil and pretilachlor, which is prepared by curing the microcapsule liquid coated with the core material;
[0055] The composition is made by the following steps:
[0056] Step S1: adding the core material and the microcapsule liquid into a stirred tank, stirring for 25 seconds at a rotating speed of 5500 r / min, and then stirring for 18 minutes at a rotating speed of 450 r / min to obtain a mixed solution;
[0057] Step S2: Add the mixed solution into the stirred tank, adjust the pH value to 5, add glutaraldehyde solution, stir for 13 minutes, and keep the temperature at 33°C for 35 minutes, filter and remove the filtrate, and dry the filter cake to prepare get the composition.
[0058] The microcapsule fluid wherein is made by following steps:
[0059] Step A1: Add tetrahydrofuran, acetophenone and phenylmagnesium bromide into the reaction kettle, and react for 5 hours under the conditions of rotation speed of 180r / min and temperature of 5...
Embodiment 3
[0068] A composition containing dipacenil and pretilachlor, which is prepared by curing the microcapsule liquid coated with the core material;
[0069] The composition is made by the following steps:
[0070] Step S1: adding the core material and the microcapsule liquid into a stirred tank, stirring for 30 seconds at a rotating speed of 6000 r / min, and then stirring for 20 minutes at a rotating speed of 500 r / min to obtain a mixed solution;
[0071] Step S2: Add the mixed solution into the stirred tank, adjust the pH value to 6, add glutaraldehyde solution, stir for 15 minutes, and keep the temperature at 35°C for 40 minutes, filter and remove the filtrate, and dry the filter cake to prepare get the composition.
[0072] The microcapsule fluid wherein is made by following steps:
[0073] Step A1: Add tetrahydrofuran, acetophenone and phenylmagnesium bromide into the reaction kettle, and react for 6 hours under the conditions of rotation speed of 200r / min and temperature of 6...
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