An implant and its preparation method and application
A technology of implants and mixtures, applied in the field of implants, can solve problems such as repeated infections, infection lesions that cannot be eradicated, and little effect
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Embodiment 1
[0099] The present embodiment prepares a kind of implant, and the specific process is:
[0100] D1. Polish and ultrasonically clean the titanium-based raw material, then place the titanium-based raw material in deionized water, ultrasonically clean it for 5 minutes, repeat three times, and air dry;
[0101] D2. Alkaline etching is performed on the titanium-based raw material obtained in step D1. The etching solution contains 4 mol / L potassium hydroxide; the reaction condition is 70° C.; the reaction time is 3 h; For deionized water, repeat three times to obtain a titanium-based substrate;
[0102] D3. get curcumin and be dispersed in deionized water to make 300 μg / mL curcumin suspension, adjust the pH of suspension to be 9, place above-mentioned suspension on magnetic stirrer and stir at uniform speed for 24h to make curcumin nanoparticle, after The particle size measured by DLS (dynamic scattering) and TEM is 150±30nm (the particle size is distributed in this range);
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Embodiment 2
[0107] The present embodiment prepares a kind of implant, and the specific process is:
[0108]D1. Polish and ultrasonically clean the titanium-based raw material; after that, place the titanium-based raw material in deionized water, ultrasonically clean for 5 minutes, repeat three times, and air dry;
[0109] D2. Alkaline etching is performed on the titanium-based raw material obtained in step D1. The etching solution contains 10 mol / L potassium hydroxide; the reaction condition is 70° C.; the reaction time is 3 h; For deionized water, repeat three times to obtain a titanium-based substrate;
[0110] D3. get curcumin and disperse it in deionized water to make a curcumin suspension of 600 μg / mL, adjust the pH of the suspension to be 8, place the above-mentioned suspension on a magnetic stirrer and stir at a uniform speed for 24h to make curcumin nanoparticles. The particle size measured by DLS (dynamic scattering) and TEM is 650±50nm (the particle size is distributed in this ...
Embodiment 3
[0115] The present embodiment prepares a kind of implant, and the specific process is:
[0116] D1. Polish and ultrasonically clean the titanium-based raw material; after that, place the titanium-based raw material in deionized water, ultrasonically clean for 5 minutes, repeat three times, and air dry;
[0117] D2. Alkaline etching is performed on the titanium-based raw material obtained in step D1. The etching solution contains 10 mol / L potassium hydroxide; the reaction condition is 70° C.; the reaction time is 3 h; For deionized water, repeat three times to obtain a titanium-based substrate;
[0118] D3. get curcumin and disperse it in deionized water to make 50 μg / mL curcumin suspension, adjust the pH of the suspension to be 7, place the above suspension on a magnetic stirrer and stir at a uniform speed for 24h to make curcumin nanoparticles. The particle size measured by DLS (dynamic scattering) and TEM is 60±5nm (the particle size is distributed in this range);
[0119]...
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