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Wear-resistant and repairable super-hydrophobic metal net and preparation method thereof

A metal mesh and super-hydrophobic technology, which is applied to the surface coating liquid device, pre-treated surface, coating, etc., can solve the problems of poor durability and irreparable surface wetting performance, and achieve good super-hydrophobic stability, The effect of excellent environmental stability and excellent friction resistance

Pending Publication Date: 2021-11-23
广东省科学院生物与医学工程研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to overcome the deficiencies of the above-mentioned prior art and provide a wear-resistant and repairable superhydrophobic metal mesh and its preparation method, by using the metal mesh as the base and modifying the surface with polydimethylsiloxane Finally, the superhydrophobic metal mesh with wear resistance and solvent resistance is prepared by using the outer flame combustion treatment, and the prepared metal mesh loses the superhydrophobic property after repeated mechanical friction, and can be burned again by the outer flame of the flame. Restoring the super-hydrophobic properties, overcoming the current disadvantages of poor durability and irreparable surface wettability of traditional metal mesh materials

Method used

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  • Wear-resistant and repairable super-hydrophobic metal net and preparation method thereof
  • Wear-resistant and repairable super-hydrophobic metal net and preparation method thereof
  • Wear-resistant and repairable super-hydrophobic metal net and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0042] A preparation method of wear-resistant and repairable superhydrophobic stainless steel mesh, such as Figure 10 As shown in the flow chart, it includes the following steps:

[0043] (1) Repeated ultrasonic cleaning with ethanol and deionized water to remove the organic pollutants and dust attached to the surface of the stainless steel mesh with a mesh number of 200 mesh stainless steel mesh;

[0044] (2) Soak the cleaned stainless steel net in n-hexane solution of polydimethylsiloxane with a solid content of 10% wt (the mass ratio of polydimethylsiloxane to curing agent is 10:1) 3 to 5 minutes, then take it out, put it in an oven at 120°C to cure for 2 hours, and obtain a stainless steel mesh whose surface is coated with polydimethylsiloxane;

[0045] (3) Burn the stainless steel mesh coated with polydimethylsiloxane on the surface for 10 s with the outer flame of an alcohol lamp to obtain a wear-resistant and repairable super-hydrophobic / super-oleophilic stainless ste...

Embodiment 2

[0049] A method for preparing a wear-resistant and repairable superhydrophobic copper mesh, comprising the steps of:

[0050] (1) Repeated ultrasonic cleaning of the copper mesh with 200 meshes with ethanol and deionized water to remove organic pollutants and dust attached to the surface of the copper mesh;

[0051] (2) Soak the cleaned copper grid in a n-hexane solution of polydimethylsiloxane with a solid content of 5% wt (the mass ratio of polydimethylsiloxane to curing agent is 10:1) 3 to 5 minutes, then take it out, put it in an oven at 80°C to cure for 2 hours, and obtain a copper mesh coated with polydimethylsiloxane on the surface;

[0052] (3) Burn the copper mesh coated with polydimethylsiloxane on the surface for 10 s with the outer flame of an alcohol lamp to obtain a wear-resistant and repairable superhydrophobic / superoleophilic copper mesh.

[0053] The superhydrophobic / superoleophilic copper mesh prepared in this example was analyzed under a scanning electron m...

Embodiment 3

[0056] A method for preparing a wear-resistant and repairable superhydrophobic stainless steel mesh, comprising the steps of:

[0057] (1) Repeated ultrasonic cleaning with ethanol and deionized water to remove the organic pollutants and dust attached to the surface of the stainless steel mesh with a mesh number of 200 mesh stainless steel mesh;

[0058] (2) Soak the cleaned stainless steel net in n-hexane solution of polydimethylsiloxane with a solid content of 15%wt (the mass ratio of polydimethylsiloxane to curing agent is 10:1) 3 to 5 minutes, then take it out, put it in an oven at 105°C to cure for 2 hours, and obtain a stainless steel mesh coated with polydimethylsiloxane on the surface;

[0059] (3) Burn the stainless steel mesh coated with polydimethylsiloxane on the surface for 10 s with the outer flame of an alcohol lamp to obtain a wear-resistant and repairable super-hydrophobic / super-oleophilic stainless steel mesh.

[0060] The superhydrophobic / superoleophilic st...

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Abstract

The invention discloses a wear-resistant and repairable super-hydrophobic metal net and a preparation method thereof. The preparation method comprises the following steps: (1) cleaning the metal net, and removing organic pollutants and dust attached to the surface; (2) soaking the cleaned metal net in an n-hexane solution of polydimethylsiloxane for 3-5 minutes, then taking out the metal net, and curing the metal net in a drying oven at 120 DEG C for 2 hours to obtain the metal net of which the surface is coated with polydimethylsiloxane; and (3) combusting the metal net with the surface coated with the polydimethylsiloxane through outer flame of flames, thereby obtaining the wear-resistant and repairable super-hydrophobic metal net. The preparation method is simple and easy to operate, reaction conditions are mild, the surface of the prepared metal net is of a good rough structure, the metal net has excellent super-hydrophobic characteristic and good durability, after the metal net loses the super-hydrophobic characteristic through repeated mechanical friction, the super-hydrophobic characteristic can be recovered only through combustion treatment of outer flames, and therefore, the method can be applied to the field of oil-water separation.

Description

technical field [0001] The invention relates to the field of functional materials, in particular to a wear-resistant and repairable super-hydrophobic metal mesh and a preparation method thereof. Background technique [0002] The frequent occurrence of marine oil spill accidents worldwide and the large amount of oily wastewater discharged in daily life and industrial processes not only pose a huge threat to the marine environment and aquatic ecosystem, but also pose a huge threat to human health. Oil-water separation is an important process for treating oil-water mixtures, so it has received extensive attention. Traditional oil-water separation methods include gravity separation, sedimentation, filtration and other methods. However, due to the low separation efficiency or complicated operation steps, the above-mentioned methods still have deficiencies in the versatility, ease of use and adaptability of oil-water separation. Therefore, how to effectively separate the oil-wat...

Claims

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Application Information

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IPC IPC(8): B05D5/00B05D5/04B05D5/08B05D7/14B05D7/24B05D3/08
CPCB05D5/00B05D5/04B05D5/08B05D7/14B05D7/24B05D3/08B05D2202/45B05D2202/15B05D2202/35
Inventor 王青谢东陈骏佳刘海露李辰
Owner 广东省科学院生物与医学工程研究所
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