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Preparation method of high-quality copper powder

A high-quality, copper powder technology, applied in metal processing equipment, transportation and packaging, etc., can solve problems such as uneven copper powder quality, achieve strong practicability, stabilize bulk density and fluidity, and reduce bridging Effect

Active Publication Date: 2022-01-07
芜湖松合新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the quality of copper powder in the process of water mist preparation is uneven. Therefore, a high-quality copper powder preparation method is designed.

Method used

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  • Preparation method of high-quality copper powder

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0028] A kind of preparation method of high-quality copper powder provides and comprises the steps:

[0029] The first step is to put the copper plate into the melting furnace for melting until it becomes copper water;

[0030] In the second step, the copper water is poured into the insulation leakage bag for atomization treatment to generate copper powder;

[0031] In the third step, the copper powder is sequentially dehydrated and dried, reduced and crushed, and screened;

[0032] In the fourth step, the finished product inspection is carried out on the copper powder after sieving.

[0033] In one embodiment, the smelting equipment includes a power frequency cored smelting furnace and an intermediate frequency cored smelting furnace, and the temperature is 1150°C to 1200°C. The atomization treatment is water atomization, the atomization time is no more than 50 minutes, and the atomization pressure is 12MPa to 14MPa; the equipment for the atomization treatment includes a hi...

Embodiment 1

[0045] see figure 1 , this example provides a preparation method of high-quality copper powder, including:

[0046] The first step is to put the copper plate into the melting furnace for melting at 1150°C until it becomes copper water;

[0047] In the second step, the copper water is poured into the thermal insulation leakage bag and atomized under the atomization pressure of 12MPa to generate copper powder;

[0048] In the third step, the copper powder is sequentially subjected to dehydration and drying treatment, screening treatment 1, reduction and crushing treatment, and sieving treatment; the temperature of the dehydration and drying treatment is 140 ° C, and the time is 100 minutes; during the drying process In the 40th minute and the 70th minute, the material was turned once, and then dried for 30 minutes; the sieving process was filtered using a 100-mesh screen; the reduction and crushing included reduction sintering and crushing, and the speed of the reduction sinterin...

Embodiment 2

[0053] see figure 1 , this example provides a preparation method of high-quality copper powder, including:

[0054] The first step is to put the copper plate into the melting furnace for melting at 1200°C until it becomes copper water;

[0055] In the second step, the copper water is poured into the thermal insulation leakage bag and atomized under the atomization pressure of 14MPa to generate copper powder;

[0056] In the third step, the copper powder is sequentially subjected to dehydration and drying treatment, screening treatment 1, reduction and crushing treatment, and sieving treatment; the temperature of the dehydration and drying treatment is 200°C; Turn the material once in the 80th minute, and then dry for 20 minutes; the sieving process uses a 100-mesh sieve to filter; the reduction and crushing includes reduction sintering and crushing, and the speed of the reduction sintering is 200mm / min. The thickness of the sintering is 30 mm, and the temperature of the redu...

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Abstract

The invention discloses a preparation method of high-quality copper powder. The preparation method comprises the following steps: 1, a copper plate is smelted in a smelting furnace for smelting until molten copper is formed; 2, the molten copper is poured into a heat preservation leakage ladle to be atomized, and copper powder is generated; 3, the copper powder is sequentially subjected to dewatering and drying treatment, reduction crushing treatment and screening treatment; and 4, the screened copper powder is subjected to finished product inspection. The smelting temperature ranges from 1150 DEG C to 1200 DEG C. The atomization treatment is water atomization, the atomization time does not exceed 50 minutes, and the atomization pressure is 12-14 MPa. The temperature of the dewatering and drying treatment is 140 DEG C to 200 DEG C. The finished product inspection comprises particle size distribution detection and fluidity detection. The method for preparing the copper powder is low in cost, convenient to popularize and high in practicability.

Description

technical field [0001] The invention relates to the field of metal materials, in particular to a preparation method of high-quality copper powder. Background technique [0002] Copper powder is widely used in powder metallurgy, electric carbon products, electronic materials, metal coatings, chemical catalysts, filters, heat pipes and other electromechanical parts and electronic aviation fields. Common copper powder preparation methods include chemical and physical methods. Chemical methods include electrodeposition, liquid phase reduction, vapor deposition, and sol-gel methods; physical methods include atomization, mechanical ball milling, and gas evaporation. Among them, the atomization method has the advantages of low production cost and less environmental pollution, so the atomization method is often used to prepare copper powder. [0003] The atomization method, also known as the spray method, uses high-speed jet gas or high-pressure water to crush the molten metal flow...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/08B22F1/14
CPCB22F9/082Y02P10/20
Inventor 孙宏园
Owner 芜湖松合新材料科技有限公司