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465results about How to "Control granularity" patented technology

Process and device for preparing graphene precursor two-dimension nanoscale graphite powder by adopting airflow crushing and peeling method

ActiveCN103977870AEasy accessCrushing and peeling is beneficialGrain treatmentsGas solidGraphene
The invention discloses a method and a device for preparing graphene precursor two-dimension nanoscale graphite powder by adopting an airflow crushing and peeling method. The device comprises an air source system, a crushing and peeling system and a gas-solid separation system; in the crushing and peeling system, an A return pipe, a B return pipe and a riser pipe form a material circulation loop of an airflow crushing and peeling process; an A gas guide pipe, a B gas guide pipe and a C gas guide pipe form an airflow crushing passage of the airflow crushing and peeling process. The graphene precursor two-dimension nanoscale graphite powder is prepared by adopting three supersonic speed jet flows to carry graphite particles together; through collision and friction of strip jet flows, high-purity crushing and peeling of the graphite particles are realized; through circulated and continuous crushing and peeling of the graphite particles, the two-dimension nanoscale graphite powder is obtained. The process is adopted for crushing and peeling the graphite powder, the crushing and peeling of the graphite powder are realized by utilizing mutual collision and friction among the graphite powder, friction of other media does not exist, and thus the two-dimension nanoscale graphite powder with high purity can be obtained.
Owner:BEIHANG UNIV

Color-magnetic separation combined sorting method for high-purity quartz sand produced through quartzite

The invention discloses a color-magnetic separation combined sorting method for high-purity quartz sand produced through quartzite. The method comprises the steps of adopting a crushing-ore washing technology to crush quartzite ore into 1.5-to-2.5 cm blocks, and carrying out ore washing through adopting a cylindrical rotating screen or a linear vibration screen; carrying out roughing and purification on the washed ore through utilizing a color sorter; after parts of a high-quality raw material are selected, carrying out ore grinding, desliming and classification; controlling the particle size of the material at 20 to 140 meshes, and carrying out secondary deironing purification on the part of material through utilizing a vertical ring pulsating high gradient magnetic separator; and after concentrating an obtained product, stacking the product, and carrying out natural dehydration to obtain the high-purity quartz sand. According to the method, adopted technologies belong to physical beneficiation, any chemical substance does not need to be added, and the method is safe and efficient to operate, good in working environment and free of tailing discharge; environmental pollution is avoided; and the method has wide application prospect in high-purity quartz sand manufacturing under the situation that high-quality ore resources are exhausted day by day.
Owner:赣州金环磁选科技装备股份有限公司

Method preparing catalyzer through liquid phase ball-milling partial reduction method and ternary copper catalyzer

The invention relates to a method preparing a copper catalyzer used for dimethyldichlorosilance synthetic reaction through a liquid phase ball-milling partial reduction method. The method includes the steps of taking copper oxide as raw material, adding solvent media containing reducing substances, enabling copper oxide particles to become small and achieve partial reduction through mechanical ball-milling, obtaining the copper-based catalyzer containing the ternary components of copper, cuprous oxide, copper oxide after suction filtration, drying and smashing, and obtaining the ternary copper catalyzer with adjustable components and controllable particles through adjusting the parameters of reducing agent types, concentration and ball-milling conditions. In catalytic reaction of organosilicone monomer synthesis, the catalyzer is high in catalytic activity and selectivity and helpful for improving the processing ability of an existing organosilicone monomer device, reduces production cost, and improves the yield of target products. The method preparing the catalyzer through the liquid phase ball-milling partial reduction method is simple in process, mild in condition and convenient to operate, and brings convenience to achieve large scale production.
Owner:JIANGXI INST OF RARE EARTHS CHINESE ACAD OF SCI

Preparation method of high-nickel, low-cobalt and low-manganese ternary positive electrode material precursor for lithium battery

The invention relates to a lithium battery preparation material, and provides a preparation method of a high-nickel, low-cobalt and low-manganese ternary positive electrode material precursor for a lithium battery. The shape and the appearance of nickel, cobalt and manganese hydroxide co-precipitated product can be precisely and conveniently controlled. A raw material solution is prepared from A, namely a nickel salt solution containing 80g/L of nickel, B, namely a mixed solution containing 60-90g/L of nickel, 10-30g/L of cobalt and 10-30g/L of manganese (prepared according to different proportions of x and y in nickel, cobalt and manganese hydroxide Ni(1-x-y)CoxMny(OH)2, wherein x is greater than or equal to 0.1 and smaller than or equal to 0.25, y is greater than or equal to 0.1 and smaller than or equal to 0.25, x+y is greater than or equal to 0.2 and smaller than or equal to 0.5), C, namely a solution containing 8mol/L of sodium hydroxide, and D, namely a solution containing a surface active dispersing agent. A preparation method comprises the steps of nickel hydroxide seed crystal cultivation, crystal particle maturing, slurry aging, precipitate filtering, washing and drying. Compared with the prior art, the preparation method has the advantages that ammonia water does not need to be added in the whole process including cultivation and confirmation of Ni(OH)2 crystals, so that high ammonia-nitrogen wastewater cannot be produced; the working procedure of treating the ammonia-nitrogen wastewater is omitted, so that the production cost is further lowered.
Owner:GANZHOU TENGYUAN COBALT INDAL

Linked data-based multiplexing method of business process execution language (BPEL) templates and services and system thereof

The invention discloses a linked data-based multiplexing method of business process execution language (BPEL) templates and services and a system thereof. The system comprises a model layer, a control layer, a user interface (UI) layer and a service asset library, wherein the model layer is used for providing models required by graphing and various functions of the whole system; the control layer is used for carrying out a control operation on a visualization process in the whole system, and further, realizing functions of script parsing of BPEL, template extracting and packaging, service combining and business exporting; the UI layer is mainly used for the functions of a palette, an editing window, an attribute view, an outline view and a guide view; and the service asset library specifically consists of field bodies, template bodies and service bodies. With the adoption of the linked data-based multiplexing method of the BPEL templates and services and the system thereof, the multi-granularity service asset multiplexing which includes the multiplexing by taking a BPEL subprocess as a template and the atomic Web service multiplexing can be realized; and the development efficiency for service combinations can be increased so as to shorten a development cycle through a pre-designed process template or a user-defined multiplexing template.
Owner:BEIJING UNIV OF POSTS & TELECOMM

Preparation method of high-whiteness high-temperature-resistance color masterbatch level titanium dioxide

The invention discloses a preparation method of high-whiteness high-temperature-resistance color masterbatch level titanium dioxide. Based on a sulfuric acid process production technology, rutile type color masterbatch special titanium dioxide is prepared through the following steps of performing sufficient rinsing, performing washing with water, performing salting, and then performing calcining so as to prepare a rutile base material free from surface treatment, wherein the rutile base material has favorable whiteness and favorable particle fineness; and performing sufficient crushing through wet grinding and sand grinding, then performing inorganic enveloping, and performing flash evaporation and drying, wherein during crushing by gas streams, organic enveloping treatment is performed, so that the high-whiteness high-temperature-resistance color masterbatch level titanium dioxide with low moisture absorption and fine particle size is prepared. The color masterbatch level titanium dioxide prepared by the preparation method disclosed by the invention can notably improve the temperature resistance situations in down-stream enterprises and the application properties of resin, and has a wide market prospect that the color masterbatch level titanium dioxide can be used for different industrial uses and can be used for manufacturing different colorful plastic articles.
Owner:SICHUAN LOMON TITANIUM IND CO LTD

Reducing reagent nozzle for denitration by SNCR method

The present invention provides a reducer nozzle used for denitration by an SNCR method. The reducer nozzle comprises a main pipe, an accessory pipe, a cutting ferrule, liquid pipes and a nozzle. The cutting ferrule is connected with the accessory pipe by screw threads to form a relative closed space. The front end of the main pipe is equipped with the nozzle and is arranged in the accessory pipe. The front end of the nozzle is contacted with the cutting ferrule. The back end of the main pipe is communicated with the liquid pipe I which is provided with a manometer. The accessory pipe is communicated with the liquid pipe II which is provided with the manometer. The nozzle is provided with a mixing hole which runs through the main pipe axially and is provided with a plurality of branch holes of the accessory which are communicated with the mixing hole and the accessory pipe. Olivary spray ports are arranged at the nozzle at a liquid outlet of the mixing hole and the cutting ferrule. The reducer nozzle has reasonable structure; when reducer penetrates an oven, the temperature range is narrow, the penetrable performance is good, and the spray distance is long; the reducer nozzle can also effectively control the granularity of atomized particles of the reducer and the vaporizing time of atomized liquid drops; and the reducer is mixed with NOx in smoke uniformly to improve the efficiency of denitrating the smoke.
Owner:JIANGSU ZHONGKE ENERGY SAVING ENVIRONMENTAL PORTECTION TECH

High-density spherical cobaltic-cobaltous oxide and method for preparing the same

The invention provides a high density spherical shape Co3O4 and a preparation method thereof, and relates to a Co3O4, in particular to the preparation of the high density spherical shape Co3O4, which is mainly used for preparing lithium cobaltoxide of anode material of a lithium ion battery, and also is used as Co3O4 of electronic grade, and belongs to the products of chemical industry. The invention provides a preparation method of the high density spherical shape Co3O4 with good fluidity, the prepared Co3O4 is enabled to be a spherical shape particle which has best stacking density and can effectively improve the tap density of the particle, thereby improving the electrochemistry property of the lithium ion battery and the quality of the lithium ion battery. The Co3O4 prepared by the method is a spherical shape crystal, the mean grain size is 5-25 micrometers, the loose packed density is more than or equal to 1.0g/cm<3>, the tap density is more than or equal to 2.0g/cm<3>, and the cobalt content is more than or equal to 73 percent. The process of the method is simple, and the lithium cobaltoxide synthesized by the Co3O4 presents better property, compared with the past Co3O4, the electrochemistry property of the lithium ion battery can be improved.
Owner:GUANGZHOU RONGJIE MATERIAL TECH

Method for preparing spherical cobalt hydroxide in the absence of complexing agent

The invention relates to a method for preparing a spherical cobalt hydroxide in the absence of a complexing agent. Though the shape of the cobalt hydroxide can be improved to a certain degree by complexing to control crystallization, the cobalt hydroxide is mostly particles in sheet shape or irregular block shape, and the addition of a complexing agent can cause negative effects. The technical scheme adopted by the invention comprises the following steps of: taking pure water as a base solution; adding a cobalt solution and a sodium hydroxide solution into the base solution with stirring at the same time to cause a precipitation reaction, wherein the pH value of the solution is kept between 5 and 7 in the process of adding the cobalt solution and the sodium hydroxide and is kept between 10.5 and 13.5 in the end of the process; adding an antioxidant into the solution to prevent the solution from being oxidized; and obtaining the cobalt hydroxide product after washing and drying the cobalt hydroxide slurry. The method adopts a forward feeding mode in the absence of complexing agent to form pink spherical cobalt hydroxide powder with very good crystallinity. The spherical cobalt hydroxide powder is easily filtered and washed, and the reaction condition is simple and easy to control. Therefore, the method is suitable for industrial mass production.
Owner:ZHEJIANG HUAYOU COBALT

Spherical manganese carbonate and preparing method thereof

The invention relates to a spherical manganese carbonate and the preparation method thereof, and mainly relates to the spherical manganese carbonate for preparing a manganese compound (manganese dioxide, etc.) of a dry battery, lithium manganese oxide of cathode materials for lithium ion batteries and derivatives, and the spherical manganese carbonate belongs to a chemical product. On the premise of easy industrial production realization, a method for simply preparing the spherical manganese carbonate with good fluidity is provided, and the spherical manganese carbonate is synthetized through controlling a synthesis technology. Particles of the manganese carbonate powder are spherical crystallization, the average particle size ranges from 2 to 30microns, the apparent density ranges from 1.3 to 1.8g per cm <3>, the tap density can reach over 2.0g per cm<3>, and the manganese content is equal to and larger than 47 percent. Experimental results indicate that the lithium manganese oxide synthetized by the manganese carbonate used as a precursor has better performance, and can improve electrochemical properties of lithium ion batteries. The lithium manganese oxide has good fluidity and highest bulk density, and can effectively improve the tap density of powder to cause materials to obtain higher specific capacity, thereby improving the electrochemical properties of the lithium ion batteries.
Owner:GUANGZHOU RONGJIE MATERIAL TECH
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