Moisture-sensitive self-adaptive breathable fabric
A self-adaptive and fabric technology, applied in textiles and papermaking, fiber treatment, liquid-repellent fibers, etc., can solve problems such as inability to make adaptive adjustments, and achieve the effect of improving wearing comfort and promoting water discharge
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0025] The preparation method of the moisture-sensitive self-adaptive breathable fabric in this embodiment comprises the following steps:
[0026] (1) Mix 0.1mol of p-chloromethylstyrene and 0.2g of 2,6-di-tert-butyl-p-methylphenol and stir for 30min until uniform, add 8.4g of pyridine, heat to 60°C for reflux reaction for 12h, and obtain a solid precipitate , the solid precipitate was washed with ether to obtain an intermediate;
[0027] (2) After mixing 10mmol of the intermediate, 11mmol of ammonium hexafluorophosphate, and 15ml of acetone, react at 30°C for 48 hours to obtain the first mixed solution, and spin-evaporate the filtrate after filtering the first mixed solution to obtain functional material monomers;
[0028] (3) Mix 2.5mmol functional material monomer, 0.025mmol copper chloride, 0.05mmol 2,2'-bipyridine, and 3ml cyclohexanone under nitrogen protection, and stir to obtain the second mixed solution;
[0029] (4) Under nitrogen protection, immerse the fabric base...
Embodiment 2
[0031] The preparation method of the moisture-sensitive self-adaptive breathable fabric in this embodiment comprises the following steps:
[0032] (1) Mix 0.3mol of p-chloromethylstyrene and 0.8g of 2,6-di-tert-butyl-p-cresol and stir for 30min until uniform, add 30g of pyridine, heat to 60°C for reflux reaction for 12h, and obtain a solid precipitate, The solid precipitate was washed with ether to obtain an intermediate;
[0033] (2) After mixing 30mmol of the intermediate, 35mmol of ammonium hexafluorophosphate, and 50ml of acetone, react at 30°C for 48 hours to obtain the first mixed solution, and spin-evaporate the filtrate after filtering the first mixed solution to obtain functional material monomers;
[0034] (3) Mix 6 mmol of functional material monomer, 0.04 mmol of copper chloride, 0.2 mmol of 2,2'-bipyridyl, and 10 ml of cyclohexanone under nitrogen protection, and stir to obtain a second mixed solution;
[0035] (4) Under nitrogen protection, immerse the fabric ba...
Embodiment 3
[0037] The preparation method of the moisture-sensitive self-adaptive breathable fabric in this embodiment comprises the following steps:
[0038] (1) Mix 0.5mol of p-chloromethylstyrene and 1.2g of 2,6-di-tert-butyl-p-cresol and stir for 40min until uniform, add 45g of pyridine, heat to 70°C for reflux for 15h, and obtain a solid precipitate, The solid precipitate was washed with ether to obtain an intermediate;
[0039] (2) After mixing 50mmol of the intermediate, 60mmol of ammonium hexafluorophosphate, and 70ml of acetone, react at 35°C for 50 hours to obtain the first mixed solution, and spin-evaporate the filtrate after filtering the first mixed solution to obtain functional material monomers;
[0040] (3) Mix 12mmol of functional material monomer, 0.15mmol of copper chloride, 0.3mmol of 2,2'-bipyridine, and 20ml of cyclohexanone under nitrogen protection, and stir to obtain a second mixed solution;
[0041] (4) Under nitrogen protection, immerse the fabric base material...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More