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Core mold material for forming rocket engine grain and preparation method of core mold material

A rocket engine and mandrel technology, applied in the field of conductive plastics, can solve the problems of high price, long processing cycle, and complex processing technology, and achieve the effects of shortening the manufacturing cycle, improving surface floating fibers, and improving surface smoothness

Pending Publication Date: 2022-02-01
HUBEI SANJIANG AEROSPACE JIANGHE CHEM TECH +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the above-mentioned technical problems, the present invention provides a light-weight high-strength mandrel material for solid rocket motor charge molding and its preparation method, which uses good matrix plastic compounding to improve matrix modulus, load high-conductive fibers and fillers Technical measures such as enhancing electrical conductivity, adjusting filler type and amount, increasing strength and reducing linear expansion coefficient can effectively solve the problems of long processing cycle, high price and complicated processing technology in alloy core molds to meet the needs of future weapon models in batches and low cost. cost, high reliability development needs

Method used

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  • Core mold material for forming rocket engine grain and preparation method of core mold material
  • Core mold material for forming rocket engine grain and preparation method of core mold material
  • Core mold material for forming rocket engine grain and preparation method of core mold material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A method for preparing a mandrel for rocket engine grain molding, comprising the following steps:

[0032] a. Plastic granulation: Measure 10kg of pure polyetherimide (PEI), 1kg of carbon nanotubes (300 mesh), 0.5kg of carbon fiber (250 mesh), 0.03kg of propyl orthosilicate, compound lubricant 0.05kg each of HyPer C100 and HBP-160, 0.3kg of diisooctyl sebacate (industrial grade), 0.02kg of 2,4-dimethyl-6-tert-butylphenol were pre-mixed, and added to the internal mixer for compaction Refining, putting the uniformly mixed material into a twin-screw extruder, the screw speed is 167rpm, heated and melted at a temperature of 217°C, and then drawn and granulated for later use;

[0033] b. Extrusion molding: heat the plastic pellets prepared in step a to 195°C through a screw rod extruder, melt and extrude them into a molding die for cooling and molding, and the size of the molding cylinder is 325*125*125mm;

[0034] c. Turning and milling of the mandrel: Carry out turning an...

Embodiment 2

[0039] A method for preparing a mandrel for rocket engine grain molding, comprising the following steps:

[0040]a. Plastic granulation: 100kg of pure polyoxymethylene (POM), 18kg of carbon nanotubes (400 mesh), 15kg of carbon fiber (300 mesh), 0.5kg of KH-560, 0.8 each of compound lubricants HyPer C181 and HBP-160 kg, 5kg of dibutyl phthalate (industrial grade), 0.5kg of 2,6-di-tert-butyl-p-cresol are pre-mixed, added to the internal mixer for internal mixing, and the evenly mixed material is put into the twin-screw Extruder, screw speed 150rpm, heating and melting at a temperature of 207°C, spinning and granulating for later use;

[0041] b. Extrusion molding: heat the pellets prepared in step a to 198°C through a screw rod extruder, melt and extrude them into a molding die for cooling and molding; the size of the molding cylinder is 800*225*225;

[0042] c. Turning and milling of the mandrel: Carry out turning and milling of the prepared cylinder according to the processin...

Embodiment 3

[0048] A method for preparing a mandrel for rocket engine grain molding, comprising the following steps:

[0049] a. Plastic granulation: 50kg of pure nylon 66 (PA66), 12.5kg of carbon nanotubes (400 mesh), 2.5kg of carbon fiber (300 mesh), 0.025kg of KH-550, compound lubricants HyPer C182 and HBP-160 0.1kg each, 0.5kg dibutyl phthalate (industrial grade), 0.4kg 2,6-di-tert-butyl-p-cresol are pre-mixed, added to the internal mixer for banburying, and banburying the uniform material Put it into a twin-screw extruder, the screw speed is 120rpm, and the temperature is 280°C, heating and melting, drawing and granulating for standby;

[0050] b. Extrusion molding: heat the pellets prepared in step a to 194°C through a screw rod extruder, melt and extrude them into a molding die for cooling and molding; the size of the molding cylinder is 325*125*125mm;

[0051] c. Turning and milling of the mandrel: Carry out turning and milling of the prepared cylinder according to the processing...

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Abstract

The invention relates to the field of conductive plastics, in particular to a core mold material for forming a rocket engine grain and a preparation method of the core mold material. The core mold material is comprises, by weight: 100 parts of a plastic pellet material; 10-25 parts of a highly conductive filler; 5-15 parts of a reinforcing filler; 0.05-0.5 part of a coupling agent; 0.2-0.8 part of a solid lubricant; 1-5 parts of a plasticizer; and 0.2-0.8 part of an antioxidant. The efficient hyperbranched lubricant containing a large number of end groups and a three-dimensional spherical structure is introduced, and the filler can be uniformly dispersed only through one-time twin-screw granulation. Meanwhile, the surface smoothness of the conductive plastic can be improved, the demolding performance is improved, and subsequent extrusion molding and processing molding are facilitated. By adopting the technical means of compounding and using good matrix plastic to improve matrix modulus, loading high-conductivity fibers and filler to enhance conductivity, adjusting the filler type and dosage to improve strength and reduce linear expansion coefficient and the like, the problems of long processing period, high price, complex processing technology and the like of an alloy core mold to a certain extent are effectively solved.

Description

technical field [0001] The invention relates to the field of conductive plastics, in particular to a core mold material used for forming rocket engine grains and a preparation method thereof. Background technique [0002] The solid rocket motor propellant grain is mainly formed by wall-mounted pouring. First, the mandrel is fixed inside the engine, and then the propellant slurry is poured on the wall. After reaching a certain strength in 7 days, it is demoulded. The propellant grains are flammable and explosive hazardous chemicals. During the demoulding process, no static electricity can be accumulated between the mandrel and the propellant grains. Resistivity (resistance value ≤1.0×106Ω.m) range belongs to electrostatic conductor. [0003] At present, alloy materials are generally used as the core mold base material. In view of the increasing size of the engine, the shape and weight of the related core mold components also increase. Even if the relatively low-density hard...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B29C43/00B29B9/06B29B7/00
CPCB29C43/00B29B9/06B29B7/00
Inventor 舒凯凯李换朝邓安华任世朝严朝雄刘海龙周安江柴枫杨松安刘佳斌
Owner HUBEI SANJIANG AEROSPACE JIANGHE CHEM TECH
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