Preparation method of aerogel warm-keeping cloth
A technology of airgel and composite airgel, which is applied in dyeing, textiles and papermaking, etc. It can solve the problems that the metal film cannot breathe and perspire, affects the flexibility of the body, and will cause stuffiness, etc., and achieves excellent thermal insulation Effects of performance, high strength, increased strength and flame retardancy
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Embodiment 1
[0025] Follow the steps below to prepare an airgel thermal cloth:
[0026] S1. Add the diabase fiber to the NaOH solution with a concentration of 2mol / L at a weight ratio of 1:25, stir for 5 minutes and transfer it to a plasma device with a discharge power of 170W for 8 minutes, take it out and wash it with deionized water To neutrality, place in a vacuum oven and dry at 100°C for 2.5 hours to obtain pretreated diabase fibers;
[0027] S2. Add ethyl orthosilicate, absolute ethanol, methyltrimethoxysilane, and DMF into deionized water, and after stirring for 10 minutes, add the pretreated diabase fiber obtained in step S1, ethyl orthosilicate, and absolute ethanol , methyltrimethoxysilane, DMF, deionized water, the ratio of the pretreated diabase fiber gained in step S1 is 1mol: 10mol: 0.5mol: 0.5mol: 200mL: 2g, with the ammoniacal liquor that is 1:50 by volume ratio Ammonia-alcoholic solution composed of absolute ethanol was adjusted to pH 8, continued to stir for 3.5 hours a...
Embodiment 2
[0032] Follow the steps below to prepare an airgel thermal cloth:
[0033] S1. Add the diabase fiber to the NaOH solution with a concentration of 2mol / L at a weight ratio of 1:25, stir for 4 minutes and then transfer it to a plasma device with a discharge power of 170W for 10 minutes, take it out and wash it with deionized water To neutrality, place in a vacuum drying oven and dry at 100°C for 2 hours to obtain pretreated diabase fibers;
[0034] S2. Add ethyl orthosilicate, absolute ethanol, methyltrimethoxysilane, and DMF into deionized water, stir for 9 minutes and then add the pretreated diabase fiber obtained in step S1, ethyl orthosilicate, and absolute ethanol , methyltrimethoxysilane, DMF, deionized water, the ratio of the pretreated diabase fiber gained in step S1 is 1mol: 10mol: 0.5mol: 0.5mol: 200mL: 2g, with the ammoniacal liquor that is 1:50 by volume ratio Ammonia-alcoholic solution composed of absolute ethanol was adjusted to pH 8, continued to stir for 3.5 hou...
Embodiment 3
[0039] Follow the steps below to prepare an airgel thermal cloth:
[0040] S1. Add the diabase fiber to the NaOH solution with a concentration of 2mol / L at a weight ratio of 1:25, stir for 4.5 minutes and then transfer it to a plasma device with a discharge power of 170W for 9 minutes, take it out and wash it with deionized water To neutrality, place in a vacuum oven and dry at 100°C for 2.5 hours to obtain pretreated diabase fibers;
[0041] S2. Add ethyl orthosilicate, absolute ethanol, methyltrimethoxysilane, and DMF into deionized water, stir for 8 minutes and then add the pretreated diabase fiber obtained in step S1, ethyl orthosilicate, and absolute ethanol , methyltrimethoxysilane, DMF, deionized water, the ratio of the pretreated diabase fiber gained in step S1 is 1mol: 10mol: 0.5mol: 0.5mol: 200mL: 2g, with the ammoniacal liquor that is 1:50 by volume ratio Ammonia-alcoholic solution composed of absolute ethanol was adjusted to pH 8, stirring was continued for 3 hour...
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