Recovery of component (c4) alkanal
A technology of alkanal and heat recovery, applied in the direction of chemical recovery, sustainable manufacturing/processing, hydrocarbon oil processing products, etc., can solve the problem of cracking facilities being shelved and unattractive
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[0680] R-thermo-hydrolyzed oil Example 1-4
[0681] Table 1 shows the composition of the R-pyrolytic oil sample by gas chromatography. The R-pyrolytic oil sample is prepared from a high and low density polyethylene, polypropylene, and polystyrene. Sample 4 is a sample of laboratory distillation, wherein the hydrocarbon greater than C21 is removed. The boiling point of these materials is shown Figure 13-16 middle.
[0682] Table 1. Gas chromatographic analysis of R-
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[0687] R-Pyrolysis Oil Example - 5-10
[0688] Six R-pyrolytic oil compositions were prepared by distillation R-thermo-hydrolyzed oil samples. They are prepared by processing materials according to the following procedures.
example 5
[0689] Example 5. R-pyrolyzed oil at least 90% at 350 ° C, 50% between 95 ° C and 200 ° C, at least 10% boiling at 60 ° C.
[0690] 250 g of the R-pyrolytic oil sample from Example 3 was distilled by 30-disc glass Oldershaw tower, which is equipped with ethylene glycol cooled condenser, a thermometer-containing thermometer sleeve and a reflow of magnets adjusted by electronic timer Controller. DC distillation is carried out at an atmospheric pressure ratio of 1: 1. The liquid fraction is collected every 20ml, record the temperature and quality of the tower to construct Figure 17 The boiling curve shown. Repeated distillation until about 635 g of substances were collected.
example 6
[0691] Example 6. At least 90% boiling at 150 ° C, 50% between 80 ° C and 145 ° C, and at least 10% boiling R-pyrolysis oil at 60 ° C.
[0692] 150 g of the R-pyrolytic oil sample from Example 3 was distilled by 30-disc glass Oldershaw tower, which is equipped with a condenser of ethylene glycol, a thermometer-containing thermometer sleeve and a reflow of magnets modulated by electronic timer. Controller. DC distillation is carried out at an atmospheric pressure ratio of 1: 1. The liquid fraction is collected every 20ml, record the temperature and quality of the tower to construct Figure 18 The boiling curve shown. Repeated distillation until about 200 g of substances were collected.
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